Specifications

Operating the Quest 21 0
Starting a Reaction
To stop the gas flow set the Manifold Control Valves as follows:
drain
solvent closed
utility
1
metered gas
vent 0 closed
utility
2
Collection of Liquid Reaction Products
When it is time to collect reaction products from the Quest, the waste container can be
removed and an appropriate collection rack installed. Position the collection rack on the
waste tray, raise the rack up until the tubes on the Lower Manifold Drain Block are
below the lip of the vials, and lock in place using the buttons on the handles.
NOTE For product collection, use the 10 psi Metered Gas, as opposed to the 30 psi
Drain Gas to provide the head pressure for fluid transfer. Using the higher pressure can
result in splashing.
Collection Rack Options
Collection racks are holders that can contain up to 20 screw top tubes or vials into which
you can collect product. The following racks are available for product collection:
A rack for 13mm x 100 mm screw cap tubes
A rack for 20 ml or 40 rnl scintillation vials
Draining Synthesis Products to the Collection Vials
- - ---- -
WARNING a During product collection, there can be a small amount of splashing.
-
Wear safety glasses, gloves, and appropriate clothing.
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