Specifications

Tm
both Manifold Control Valves to "CLOSED"
Drain Gas Metered Gas
Solvent Closed Vent
@-
Closed
Utility
1
Utility
2
Unscrew the Solvent Bottle Cap from the
4
L
bottle.
Wipe off any residual solvent on the Solvent Bottle Pick-Up Line.
Dispose of the white polyethylene SolventIReagent Inlet Filter and install a new one
on the end of the Solvent Bottle Pick-Up Line.
Replace the
4
L
solvent bottle in the Safety Container with a
4
L
bottle of DCM.
Take care not to misplace the Teflon bottle seal.
Remove the cap from the DCM bottle. Insert the Teflon bottle seal into the neck of
the DCM bottle. Screw the bottle cap assembly on hand tight. Turn the black valve
on top of the Solvent Bottle Cap towards the tubing marked "Bottle Pressure". Wait
-1
minute for the bottle to pressurize.
Parallel Delivery of Methylene Chloride to
RVs
for ArgoCap Washing
To deliver DCM to
10
RVs in parallel, "pressurize" the bottle of DCM and "vent" the
RVs by turning the Manifold Control Valves to "SOLVENT" and "VENT". When
Drain Gas Metered Gas
Solvent Closed Vent
0
Closed
Utility
1
Utility
2
the solvent has reached the top row of screws on the spring-loaded insulators on the
front of the Reactor Unit (RV is
314
fill,
-4
mL), purge the manifold by
slowly
turning the left Manifold Control Valve from "SOLVENT" to "DRAIN GAS".
Allow the Upper Manifold to purge for
-5
seconds. Purging the Upper Manifold will
chase residual solvent into the RVs using nitrogen gas.
Drain Gas Metered Gas
Utility
1
Argonaut Technologl~s
Part
Number 102298
Vent
G
Closed
Utility
2
04/02/98
Quest
Tutorial
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