Instruction Manual PN 51-1055pHC/rev.
ESSENTIAL INSTRUCTIONS WARNINGS READ THIS PAGE BEFORE PROCEEDING! RISK OF ELECTRICAL SHOCK Your purchase from Rosemount Analytical, Inc. has resulted in one of the finest instruments available for your particular application. These instruments have been designed, and tested to meet many national and international standards. Experience indicates that its performance is directly related to the quality of the installation and knowledge of the user in operating and maintaining the instrument.
QUICK START GUIDE FOR MODEL SOLU COMP II pH/CONDUCTIVITY ANALYZER (Model Option 1055-22-30) 1. Refer to Section 2.0 for installation instructions. 2. Wire sensor(s) to the analyzer. See the drawings below. Refer to the sensor instruction sheet for details. Make alarm and output connections as shown below. NOTE For sensors without solution ground, please use the RC kit included with the instrument.
. When the analyzer is powered up for the first time, Quick Start screens appear. Using Quick Start is easy. a. A blinking field shows the position of the cursor. b. Use the or key to move the cursor left or right. Use the or key to move the cursor up or down or to increase or decrease the value of a digit. Use the or key to move the decimal point. c. Press ENTER to store a setting. Press EXIT to leave without storing changes. Pressing EXIT also returns the display to the previous screen.
pH/cond/temp MENU TREE FOR pH/ORP/REDOX/CONDUCTIVITY/RESISTIVITY/TDS MEASUREMENTS QUICK REFERENCE GUIDE
MODEL SOLU COMP II TABLE OF CONTENTS MODEL SOLU COMP II DUAL INPUT pH/CONDUCTIVITY ANALYZER TABLE OF CONTENTS Section Title Page 1.0 DESCRIPTION AND SPECIFICATIONS ................................................................ 1 1.1 Features and Applications........................................................................................ 1 1.2 Specifications ........................................................................................................... 2 1.
MODEL SOLU COMP II TABLE OF CONTENTS TABLE OF CONTENTS CONT’D Section Title Page 6.0 CALIBRATION ........................................................................................................ 45 6.1 Introduction .............................................................................................................. 45 6.2 Calibrating Temperature........................................................................................... 46 6.
MODEL SOLU COMP II TABLE OF CONTENTS LIST OF FIGURES Number Title Page 2-1 Panel Mount Installation ........................................................................................... 2-2 Pipe Mount Installation ............................................................................................. 13 2-3 Surface Mount Installation ........................................................................................ 14 3-1 Removing the Knockouts ................................
About This Document This manual contains instructions for installation and operation of the Solu Comp II Model 1055 Dual Input pH/Conductivity Analyzer. The following list provides notes concerning all revisions of this document. Rev. Level Date 0 1/01 This is the initial release of the product manual. The manual has been reformatted to reflect the Emerson documentation style and updated to reflect any changes in the product offering. A 2/02 Revised specs. B 7/02 Added 399 wiring diagrams.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS SECTION 1.0. DESCRIPTION AND SPECIFICATIONS 1.1 FEATURES AND APPLICATIONS 1.2 SPECIFICATIONS 1.3 ORDERING INFORMATION AND ACCESSORIES 1.1 FEATURES AND APPLICATIONS The Solu Comp II analyzers offer the choice of single or dual sensor input with measurement choices of pH/ORP, resistivity/conductivity/TDS, % concentration, ratio conductivity, total and free chlorine, dissolved oxygen, dissolved ozone, flow and temperature.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS 1.2 SPECIFICATIONS - General Case: ABS (panel-mount), polycarbonate (pipe- and surface-mount). All versions are NEMA 4X/CSA 4 (IP65). Dimensions Panel (code -10): 6.10 x 6.10 x 3.72 in. (155 x 155 x 94.5 mm) Surface/Pipe (code -11): 6.23 x 6.23 x 3.23 in. (158 x 158 x 82 mm); see page 5 for dimensions of pipe mounting bracket. Conduit openings: Accepts PG13.5 or 1/2 in. conduit fittings Display: Two line, 16-character, back-lit display.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS CONTACTING CONDUCTIVITY (Codes -20 and/or -30) Measures conductivity in the range 0 to 20,000 µS/cm. Display choices are conductivity, resistivity, and TDS (total dissolved solids). Three temperature corrections are available: high purity water (dilute sodium chloride), cation conductivity (dilute hydrochloric acid), and adjustable linear temperature coefficient (0 to 5.00%/°C).
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS TOROIDAL CONDUCTIVITY (Codes -21 and/or -31) When used with Model Series 200 Toroidal Conductivity Sensors, display choices are conductivity, resistivity, and percent concentration. The percent concentration selection includes the choice of four common solutions (0-12% NaOH, 0-15% HCl, and 0-25% or 96-99.7% H2SO4). The conductivityconcentration algorithms for these solutions are fully temperature compensated.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS pH/ORP (Codes -22 and/or -32) For use with any standard pH or ORP sensor and all Uniloc sensors and junction boxes with built-in diagnostic style preamplifiers, display choices are pH, ORP or Redox. The automatic buffer recognition feature uses stored buffer values and their temperature curves for the most common buffer standards available worldwide.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS FLOW (Standard on all models or stand alone, Code -23 and/or -33) For use with most pulse signal flow sensors, the Solu Comp II's user selectable units of measure include flow rates in GPM (Gallon per minute), LPM (liters per minute), or m3/hr (cubic meters per hour), and velocity in ft/sec or m/sec. When configured to measure flow, the unit also acts as a totalizer in the chosen unit (gallons, liters, or cubic meters).
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS DISSOLVED OXYGEN (Code -25) When used with an oxygen permeable membranecovered amperometric sensor, display choices are ppb or ppm dissolved oxygen or % saturation. Because the permeability of the membrane is a function of temperature, a correction is necessary when the sensor is used at a temperature different from the one at which it was calibrated. The Solu Comp II automatically applies the temperature correction factor.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS 1.3 ORDERING INFORMATION The Solu Comp II analyzers offer the choice of single or dual sensor input with measurement choices of pH/ORP, conductivity/resistivity, toroidal conductivity, flow, chlorine, dissolved oxygen, and dissolved ozone. See combination guide (on the following page) for valid combinations. Standard features include two isolated outputs, three alarm relays, customizable two-line display, and temperature correction.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS COMBINATION GUIDE 5 5 * For D.O. sensors with 22k thermistor, use Suite 1 only.
MODEL SOLU COMP II SECTION 1.0 DESCRIPTION AND SPECIFICATIONS ACCESSORIES (Weights are rounded up to nearest whole lb or 0.5 kg) PART NUMBER DESCRIPTION WEIGHT SHIPPING WT. 23820-00 Pipe mounting kit, includes U-bolts, mounting bracket, nuts, washers, and screws (complete) 2 lb (1.0 kg) 4 lb (2.0 kg) 23554-00 Gland fittings, PG 13.5, 5 per package 1 lb (0.5 kg) 2 lb (1.0 kg) 9240048-00 Tag, stainless steel (specify marking) 1 lb (0.5 kg) 1 lb (0.5 kg) pH INPUT 9210012 Buffer Solution, 4.
MODEL SOLU COMP II SECTION 2.0 INSTALLATION SECTION 2.0. INSTALLATION 2.1 UNPACKING AND INSPECTION 2.2 INSTALLATION 2.1 UNPACKING AND INSPECTION Inspect the shipping container. If it is damaged, contact the shipper immediately for instructions. Save the box. If there is no apparent damage, unpack the container. Be sure all items shown on the packing list are present. If items are missing, notify Rosemount Analytical immediately. 2.2 INSTALLATION 2.2.1 General Information 1.
MODEL SOLU COMP II SECTION 2.0 INSTALLATION 2.2.2 Panel Mounting. MILLIMETER INCH FIGURE 2-1. Panel Mount Installation Access to the wiring terminals is through the rear cover. Four screws hold the cover in place.
MODEL SOLU COMP II SECTION 2.0 INSTALLATION 2.2.3 Pipe Mounting. MILLIMETER INCH FIGURE 2-2. Pipe Mount Installation The front panel is hinged at the bottom. The panel swings down for access to the wiring terminals.
MODEL SOLU COMP II SECTION 2.0 INSTALLATION 2.2.4 Surface Mounting. MILLIMETER INCH FIGURE 2-4. Surface Mount Installation The front panel is hinged at the bottom. The panel swings down for access to the wiring terminals.
MODEL SOLU COMP II SECTION 3.0 WIRING SECTION 3.0. WIRING 3.1 PREPARING CONDUIT OPENINGS 3.2 POWER, ALARM, OUTPUT, AND SENSOR CONNECTIONS 3.1 PREPARING CONDUIT OPENINGS The number of conduit openings and the location depend on the model. Model 1055-10 1055-11 Description panel mount surface or pipe mount Conduit openings two open, three knockouts three open, no knockouts Conduit openings accept 1/2-inch conduit fittings or PG 13.5 cable glands.
MODEL SOLU COMP II SECTION 3.0 WIRING FIGURE 3-2. Wiring Connections for Solu Comp II Model 1055-01-10 (Panel Mount with 115/230 Vac Power) FIGURE 3-3.
MODEL SOLU COMP II SECTION 3.0 WIRING FIGURE 3-4. Wiring Connections for Solu Comp II Model 1055-01-11 (Surface/Pipe Mounting with 115/230 Vac Power) FIGURE 3-5.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055105 B FIGURE 3-6. Panel Mount Wiring to Models 399-09-62, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055106 B FIGURE 3-7. Pipe/Wall Mount Wiring to Models 399-14, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055107 B FIGURE 3-8. Pipe/Wall Mount Wiring to Models 399VP-09, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055108 B FIGURE 3-9. Panel Mount Wiring to Models 399VP-09, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055109 B FIGURE 3-10. Pipe/Wall Mount Wiring to Models 399-09-62, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II DWG. NO. SECTION 3.0 WIRING REV. 41055110 B FIGURE 3-11. Panel Mount Wiring to Models 399-14, 400, 401, 402, 403, and 404.
MODEL SOLU COMP II SECTION 3.0 WIRING DWG. NO. 40105536 FIGURE 3-12. Wiring Model 1055-11-22-32 to Models 399-09-62 and GP-1. 24 REV.
MODEL SOLU COMP II SECTION 3.0 WIRING DWG. NO. REV. 40105559 E FIGURE 3-13. Wiring Model 1055-10-22-32 to Model 399-14 DWG. NO. 41055112 REV. C FIGURE 3-14.
MODEL SOLU COMP II SECTION 4.0 DISPLAY AND OPERATION SECTION 4.0 DISPLAY AND OPERATION 4.1 4.2 4.3 4.4 4.5 DISPLAY KEYPAD PROGRAMMING AND CALIBRATING THE SOLU COMP II - TUTORIAL SECURITY USING HOLD 4.1. DISPLAY The Solu Comp II has a two-line display. The display can be customized to meet user requirements (see Section 5.11). Figure 4-1 shows some of the displays available during normal operation. View A is the default screen for a dual sensor. View B is the default screen for a single sensor.
MODEL SOLU COMP II SECTION 4.0 DISPLAY AND OPERATION 4.3 PROGRAMMING AND CALIBRATING THE SOLU COMP II - TUTORIAL Setting up and calibrating the Solu Comp II is easy. The following tutorial describes how to move around in the programming menus. For practice, the tutorial also describes how to assign conductivity values to the 4 and 20 mA outputs for sensor 1. Calibrate Program Calibrate Hold Display Hold Program Display Outputs Alarms Measurement >> 1.
MODEL SOLU COMP II SECTION 4.0 DISPLAY AND OPERATION 4.4 SECURITY 4.4.1 How the Security Code Works Use the security code to prevent accidental or unwanted changes to program settings, displays, and calibration. Enter Security 000 Code 1. If a security code has been programmed, pressing MENU causes the security screen to appear. 2. Enter the three-digit security code. Invalid Code 3. If the entry is correct, the main menu screen appears. If the entry is incorrect, the Invalid Code screen appears.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER SECTION 5.0 PROGRAMMING THE ANALYZER 5.1 5.2 5.3 5.4 5.5 GENERAL CHANGING STARTUP SETTINGS CONFIGURING AND RANGING THE OUTPUTS CONFIGURING ALARMS AND ASSIGNING SETPOINTS SELECTING THE TYPE OF MEASUREMENT AND ACTIVATING SOLUTION TEMPERATURE CORRECTION 5.6 CHOOSING TEMPERATURE UNITS AND MANUAL OR AUTOMATIC TEMPERATURE COMPENSATION 5.7 SETTING A SECURITY CODE 5.8 NOISE REJECTION 5.9 SINGLE SENSOR OR DUAL SENSOR INPUT 5.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER TABLE 5-1. DEFAULT SETTINGS 1. SENSOR-OUTPUT ASSIGNMENTS (pH, ORP, redox, conductivity, resistivity, or TDS is selected during Quick Start) Sensor(s) Output 1 Output 2 Section Single sensor pH/ORP/Redox Temperature 5.3 and 5.9 Dual sensor pH/ORP/Redox (sensor 1) Conductivity/Resistivity (sensor 2) 5.3 and 5.9 2. OTHER OUTPUT SETTINGS Output Dampening 0 or 4 mA Mode Section 1 off 4 Linear 5.3 2 off 4 Linear 5.3 3.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER TABLE 5-1. DEFAULT SETTINGS (continued) 5. TEMPERATURE RELATED SETTINGS Section Units °C 5.6 Automatic temperature compensation (pH) On 5.6 Automatic temperature correction (conductivity) On 5.6 Solution temperature correction (pH) Off 5.5 Isopotential pH 7.00 5.5 Temperature correction (conductivity) neutral salt 5.5 Temperature slope 2%/°C 5.5 6. MISCELLANEOUS SETTINGS Section Language English 5.11 Hold off 4.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.3 CONFIGURING AND RANGING THE OUTPUTS. 5.3.1 Purpose The Solu Comp II accepts input from a pH, ORP, or conductivity sensor and has two current outputs. This section describes how to configure and range the outputs. CONFIGURE THE OUTPUTS FIRST. 1. Configuring an output means a. Selecting either a 4-20 mA or 0-20 mA output, b.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.3.3. Procedure: Configure Outputs. To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms Measurement 1. Press MENU. The main menu screen appears. Choose Program. 2. Choose Outputs. >> 3. Choose Output Configure. Output Range Output Configure 4. Choose Output1 or Output2.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.4 CONFIGURING ALARMS AND ASSIGNING SETPOINTS 5.4.1 Purpose This section describes how to do the following: 1. assign an alarm relay to a sensor, 2. set the alarm logic to high or low, 3. assign values to the alarm setpoints, 4. set the alarm deadbands. ALARM RELAYS MUST BE CONFIGURED BEFORE ASSIGNING SETPOINTS. 5.4.2 Definitions 1. ASSIGNING ALARMS. There are three alarms (AL1, AL2, and AL3). Alarms 1 and 2 can be assigned to any sensor.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.4.3 Procedure: Configuring Alarms To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms Measurement 1. Press MENU. The main menu screen appears. Choose Program. 2. Choose Alarms. >> 3. Choose Alarm Configure. Alarm Setpoints Alarm Configure 4. Choose Alarm 1 (AL1), Alarm 2 (AL2), or Alarm 3 (AL3). Alarm Config? AL1 AL2 AL3 5.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.4.4 Procedure: Programming Alarm Setpoints To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms Measurement 1. Press MENU. The main menu screen appears. Choose Program. 2. Choose Alarms. >> Alarm Setpoints 3. Choose Alarm Setpoints. Alarm Configure 4. Choose Alarm 1 (AL1), Alarm 2 (AL2), or Alarm 3 (AL3).
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.5 SELECTING THE TYPE OF MEASUREMENT AND ACTIVATING SOLUTION TEMPERATURE CORRECTIONS 5.5.1 Purpose This section describes how to do the following: 1. Program the Solu Comp II to measure pH, ORP, redox potential, conductivity, resistivity, or total dissolved solids. 2. Enable or disable glass impedance fault. 3. Select a solution temperature correction for pH. 4. Change the analyzer pH isopotential point. 5.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.5.3 Definitions — conductivity/resistivity 1. NEUTRAL SALT CORRECTION. Neutral salt temperature correction is appropriate for most applications involving natural and treated waters in which neutral salts are primarily responsible for the conductivity. It is NOT suitable if the sample is a dilute acid or base.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.5.4 Procedure. To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms Measurement 1. Press MENU. The main menu screen appears. Choose Program. 2. Choose Measurement. >> Config? Sensor1 Sensor2 3. Choose Sensor 1 (pH) or Sensor 2 (conductivity). For a single input configuration, the Sensor 1 Sensor 2 screen does not appear.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.6 CHOOSING TEMPERATURE UNITS AND MANUAL OR AUTOMATIC TEMPERATURE COMPENSATION 5.6.1 Purpose This section describes how to do the following: 1. Choose temperature display units (°C or °F). 2. Choose automatic or manual temperature compensation for pH. 3. Choose automatic or manual temperature correction for conductivity/resistivity. 4. Enter a temperature for manual temperature compensation. 5.6.2 Definitions — pH 1.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.6.4 Procedure. To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms 2. Choose >>. >> Measurement Temp Security #Sensors 3. Choose Temp. >> Config Temp? °C/F 1. Press MENU. The main menu screen appears. Choose Program. Live/Manual 4. Choose °C/F to change temperature units.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.8 NOISE REJECTION 5.8.1 Purpose. For maximum noise rejection, the frequency of the ac power must be entered in the analyzer. 5.8.2. Procedure. To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. Calibrate Hold Program Display Outputs Alarms Measurement 2. Choose >>. >> Temp Security #Sensors 3. Choose >>. >> Noise Rejection ResetAnalyzer 1. Press MENU.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER 5.10 RESETTING FACTORY CALIBRATION AND FACTORY DEFAULT SETTINGS 5.10.1 Purpose. This section describes how to re-install factory calibration and default values. The process also clears all fault messages and returns the display to the first quick start screen. 5.10.2. Procedure. To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER.
MODEL SOLU COMP II SECTION 5.0 PROGRAMMING THE ANALYZER To choose a menu item, move the cursor to the item and press ENTER. To store a number or setting, press ENTER. 5.11.2 Procedure: Selecting a Display Screen Calibrate Hold 1. Press MENU. The main menu screen appears. Choose Display. Display Program 2. Choose Default Display. Default Display Language Contrst 3. Press or until the desired display appears. Press ENTER. For an explanation of abbreviations, see Section 5.11.1. 4.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION SECTION 6.0 CALIBRATION 6.1 6.2 6.3 6.4 6.5 6.6 6.7 6.8 6.9 6.10 INTRODUCTION CALIBRATING TEMPERATURE AUTO CALIBRATION - pH MANUAL CALIBRATION - pH STANDARDIZATION - pH ENTERING A KNOWN SLOPE - pH ORP CALIBRATION CALIBRATING AN IN-SERVICE SENSOR - CONDUCTIVITY PLACING A NEW SENSOR IN SERVICE - CONDUCTIVITY CALIBRATING THE ANALYZER - CONDUCTIVITY 6.1 INTRODUCTION The Calibrate Menu allows the user to calibrate sensor 1 (pH or ORP) and sensor 2 (conductivity).
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.2 CALIBRATING TEMPERATURE 6.2.1 Purpose Temperature is important in the measurement of pH, ORP, and conductivity (or resistivity) for different reasons. Temperature affects the measurement of pH in three ways. 1. The analyzer uses a temperature dependent factor to convert measured cell voltage to pH. Normally, a slight inaccuracy in the temperature reading is unimportant unless the pH reading is significantly different from 7.00. Even then, the error is small.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.2.2 Procedure 1. Remove the sensor from the process. Place it in an insulated container of water along with a calibrated thermometer. Submerge at least the bottom two inches of the sensor. Stir continuously. 2. Allow the sensor to reach thermal equilibrium. For some sensors, the time constant for a change in temperature is 5 min., so it may take as long as 30 min. for temperature equilibration. 3.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.3 AUTO CALIBRATION — pH 6.3.1 Purpose 1. New sensors must be calibrated before use. Regular recalibration is also necessary. 2. Use auto calibration instead of manual calibration. Auto calibration avoids common pitfalls and reduces errors. 6.3.2 Definitions 1. AUTO CALIBRATION. The analyzer recognizes the buffers and uses temperature-corrected pH values in the calibration. The table lists the buffers the Solu Comp II recognizes.
MODEL SOLU COMP II Calibrate Program SECTION 6.0 CALIBRATION Hold Calibrate? Sensor1 b. Choose Sensor1 (pH sensor). Sensor2 c. CalSensor1? Measurement S1 Slope Standardize d. Choose BufferCal. BufferCal e. Choose Auto. Manual f. S1AutoCal? Buffer1 Choose Measurement. Temp S1BufferCal? Auto a. Press MENU. The main menu screen appears. Choose Calibrate. Display Choose Buffer1. Buffer2 g. Rinse the sensor with water and place it in buffer 1.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.4 MANUAL CALIBRATION — pH 6.4.1 Purpose 1. New sensors must be calibrated before use. Regular recalibration is also necessary. 2. Use manual calibration if non-standard buffers are being used; otherwise, use auto calibration. Auto calibration avoids common pitfalls and reduces errors. 6.4.2 Definitions 1. MANUAL CALIBRATION. In auto calibration the analyzer recognizes the buffer and uses the temperature-corrected pH value in the calibration.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION Calibrate Program Hold Calibrate? Sensor1 b. Choose Sensor1 (pH sensor). Sensor2 c. CalSensor1? Measurement S1 Slope Choose Measurement. Temp Standardize d. Choose BufferCal. BufferCal e. Choose Manual. S1BufferCal? Manual Auto f. S1ManualCal? Buffer1 a. Press MENU. The main menu screen appears. Choose Calibrate. Display Choose Buffer1. Buffer2 g. Rinse the sensor with water and place it in buffer 1.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.5 STANDARDIZATION — pH 6.5.1 Purpose 1. The pH measured by the Solu Comp II analyzer can be changed to match the reading from a second or referee instrument. The process of making the two readings agree is called standardization. 2. During standardization, the difference between the two pH values is converted to the equivalent voltage. The voltage, called the reference offset, is added to all subsequent measured cell voltages before they are converted to pH.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.6 ENTERING A KNOWN SLOPE VALUE — pH 6.6.1 Purpose If the electrode slope is known from other measurements, it can be entered directly in the Solu Comp II analyzer. The slope must be entered as the slope at 25°C. To calculate the slope at 25°C from the slope at temperature t°C, use the equation: 298 slope at 25°C = (slope at t°C) t°C + 273 Changing the slope overrides the slope determined from the previous buffer calibration. 6.6.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.7 ORP CALIBRATION 6.7.1 Purpose 1. For process control, it is often important to make the measured ORP agree with the ORP of a standard solution. 2. During calibration, the measured ORP is made equal to the ORP of a standard solution at a single point. 6.7.2 Preparation of ORP standard solutions ASTM D1498-93 gives procedures for the preparation of iron (II) - iron (III) and quinhydrone ORP standards. The iron (II) - iron (III) standard is recommended.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.8 CALIBRATING AN IN-SERVICE SENSOR — CONDUCTIVITY 6.8.1 Purpose 1. After a conductivity sensor has been in service for a period of time, recalibration may be necessary. 2. There are three ways to calibrate a sensor. a. Use a standard instrument and sensor to measure the conductivity of the process stream. It is not necessary to remove the sensor from the process piping. See Figure 6-2.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION Calibrate Hold Program Display Outputs Alarms Measurement b. Choose Measurement. >> c. Configure? Sensor1 Choose Sensor2 (conductivity). Sensor2 Cond S2 Measure? TDS d. Choose Cond. Resistivity e. Choose Other. S2 Temp Corr? NeutSalt Other S2 Temp Corr? Slope a. Press MENU. The main menu screen appears. Choose Program. f. Cation Choose Raw. Raw g. The display returns to the screen in step c.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION Possible Cal Error Proceed? Yes Updated S2 Cell No h. If the change is more than 10% of the present value, the Solu Comp II displays a warning screen. Choose Yes to have the analyzer accept the calibration. Choose No to repeat the calibration. Go to steps i through k. i. After the calibration is accepted, the updated cell constant screen appears for about 5 seconds. j. The display returns to the screen in step b.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION Calibrate Hold Program Display Outputs Alarms Measurement b. Choose Measurement. >> c. Configure? Sensor1 Choose Sensor2 (conductivity). Sensor2 Cond S2 Measure? TDS d. Choose Cond. Resistivity e. Choose Other. S2 Temp Corr? NeutSalt Other f. S2 Temp Corr? Slope a. Press MENU. The main menu screen appears. Choose Program. Cation Choose Raw. Raw g. The display returns to the screen in step c.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION Possible Cal Error Yes Proceed? No Updated S2 Cell h. If the change is more than 10% of the present value, the Solu Comp II displays a warning screen. Choose Yes to have the analyzer accept the calibration. Choose No to repeat the calibration. Go to steps i through k. i. After the calibration is accepted, the updated cell constant screen appears for about 5 seconds. j. The display returns to the screen in step b.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 6.10 CALIBRATING THE ANALYZER - CONDUCTIVITY. 6.10.1 Purpose 1. After a conductivity analyzer has been in service for a period of time recalibration may be necessary. 2. To check the calibration of the Solu Comp II, see Section 8.7. If the calibration does not meet specifications, the analyzer can be recalibrated according to Section 6.10.2. 3.
MODEL SOLU COMP II SECTION 6.0 CALIBRATION 4. Choose Sensor2 (conductivity sensor). Calibrate? Sensor1 Sensor2 5. Choose Measurement. Cal Sensor2? Measurement Temp CalS2? InProcess Meter CellConst 6. Choose Meter. 7. The information screen shown at left appears momentarily. Use precision resistors only Live 50.00k^ Input1 50.00k^ 8. The first line is the live resistance reading. Change the number in the second line to match the true resistance. Resistance must be entered in units of kΩ.
MODEL SOLU COMP II SECTION 7.0 MAINTENANCE SECTION 7.0 MAINTENANCE 7.1 OVERVIEW 7.2 REPLACEMENT PARTS 7.1 OVERVIEW The Solu Comp II analyzer needs little routine maintenance. The calibration of the analyzer and sensor should be checked periodically. To recalibrate the analyzer and sensor, see Section 6.0. Clean the analyzer case and front panel by wiping with a clean soft cloth dampened with water ONLY. Do not use solvent, like alcohol, that might cause a buildup of static charge. 7.
MODEL SOLU COMP II SECTION 7.0 MAINTENANCE TABLE 7-1. Replacement Parts for Solu Comp II (Panel Mount Version) Location in Figure 7-1 PN 1 23823-00 Panel mounting kit, includes four brackets and four set screws 2 lb/1.0 kg 2 23837-00 Enclosure, front, for panel mount version, includes keypad 3 lb/1.0 kg 3 33654-00 Gasket, front, for panel mount version 2 lb/1.0 kg 4 note 5 23822-00 6 note PCB, microprocessor 7 note Screw, self-tapping, #4 x 0.375 in.
MODEL SOLU COMP II SECTION 7.0 MAINTENANCE TABLE 7-2. Replacement Parts for Solu Comp II (Pipe/Surface Mount Version) Location in Figure 7-2 PN Description Shipping Weight 1 note Screw, 6-32 x 1.38 in. 2 note Washer 3 23834-00 Enclosure, front, for pipe/surface mount version, includes keypad and hinge 2 lb/1.0 kg 4 33655-00 Gasket for pipe/surface mount version 2 lb/1.0 kg 5 note 6 23822-00 7 note PCB, microprocessor 8 note Self-tapping screw, #4 x 0.375 in.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING SECTION 8.0 TROUBLESHOOTING 8.1 OVERVIEW 8.2 TROUBLESHOOTING USING FAULT CODES 8.3 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING — pH 8.4 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING — CONDUCTIVITY 8.5 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING — GENERAL 8.6 SIMULATING INPUTS — pH 8.7 SIMULATING INPUTS — CONDUCTIVITY 8.8 SIMULATING TEMPERATURE 8.9 MEASURING REFERENCE VOLTAGE — pH 8.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.2.2 pH Sensitive Glass Membrane is Broken The Solu Comp II continuously measures the impedance between the sensor solution ground and the inside of the pH-sensing electrode. If the glass membrane is intact, the impedance is normally between 10 MΩ and 1000 MΩ. If the membrane is cracked or broken, the impedance drops below 10 MΩ. If the membrane is cracked or broken, the sensor must be replaced. 8.2.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.3 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING — pH. Problem See Section New temperature during calibration more than 2-3°C different from the live reading 8.3.1 Calibration Error warning during two-point calibration 8.3.2 Calibration Error warning during standardization 8.3.3 Invalid Input while manually entering slope 8.3.4 Sensor does not respond to known pH changes 8.3.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING REFERENCE IMPEDANCE (Ref Imp) less than 40 kΩ (20 kΩ for TUpH sensors) Normal reading, reference junction is clean. between 40 and 140 kΩ (20 - 140 kΩ for TUpH sensors) Reference junction is fouled or dirty. greater than 140 kΩ Reference junction is blocked or electrolyte is depleted. Sensor has failed. GLASS IMPEDANCE (Glass Imp) less than 10 MΩ Glass bulb is cracked or broken. Sensor has failed. between 10 and 1000 MΩ Normal reading.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.3.7 Calibration Was Successful, but Process pH Is Grossly Wrong and/or Noisy. Grossly wrong or noisy readings suggest a ground loop (measurement system connected to earth ground at more than one point), a floating system (no earth ground), or noise being brought into the analyzer by the sensor cable. The problem arises from the process or installation. It is not a fault of the analyzer.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.4 TROUBLESHOOTING WHEN NO ERROR MESSAGE IS SHOWING — CONDUCTIVITY Problem See Section Calibration Error using standard resistors 8.4.1 New temperature during calibration more than 2-3°C different from the live reading 8.4.2 Possible Error Warning during calibration against standard solutions 8.4.3 Possible Error Warning during calibration against standard meter and cell 8.4.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.4.5 Measurement seems wrong. A. If sensor is being installed for the first time, check the wiring connections. See Section 3.2. B. Verify that the sensor is completely immersed in the process liquid. C. Be sure the sensor has a cell constant appropriate for the liquid being measured. Refer to the table below. Conductivity, µS/cm Cell constant, /cm 0.0 - 50 0.01 5 - 500 0.10 50 - 5000 1.0 500 - 20,000 10 D.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.6 SIMULATING INPUTS — pH 8.6.1 General This section describes how to simulate a pH input into the Solu Comp analyzer. To simulate a pH measurement, connect a standard millivolt source to the transmitter. If the transmitter is working properly, it will accurately measure the input voltage and convert it to pH. Although the general procedure is the same, the wiring details depend on the location of the preamplifier. 8.6.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.7 SIMULATING INPUTS — CONDUCTIVITY To check the performance of the analyzer, use standard resistors to simulate conductivity. A. Set the temperature correction to raw (Section 5.5). B. Connect the standard resistors to TB-5 as shown in Figure 8-4. C. Determine how closely the displayed resistivity or conductivity agrees with the known resistance.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.8 SIMULATING TEMPERATURE 8.8.1 General. The Solu Comp II accepts either a Pt100 or a Pt1000 RTD in a three-wire configuration. See Figure 8-5. 8.8.2 Simulating temperature To simulate the temperature input, wire a decade box to the analyzer or junction box as shown in Figure 8-6. To check the accuracy of the temperature measurement, set the resistor simulating the RTD to the values indicated in the table and note the temperature readings.
MODEL SOLU COMP II SECTION 8.0 TROUBLESHOOTING 8.9 MEASURING REFERENCE VOLTAGE Some processes contain substances that poison or shift the potential of the reference electrode. Sulfide is a good example. Prolonged exposure to sulfide converts the reference electrode from a silver/silver chloride electrode to a silver/silver sulfide electrode. The change in reference voltage is several hundred millivolts.
MODEL SOLU COMP II SECTION 9.0 RETURN OF MATERIAL SECTION 9.0 RETURN OF MATERIAL 9.1 9.2 9.3 GENERAL WARRANTY REPAIR NON-WARRANTY REPAIR 9.1 GENERAL. To expedite the repair and return of instruments, proper communication between the customer and the factory is important. Before returning a product for repair, call 1-949-757-8500 for a Return Materials Authorization (RMA) number. 9.2 WARRANTY REPAIR. The following is the procedure for returning instruments still under warranty: 1.
WARRANTY Seller warrants that the firmware will execute the programming instructions provided by Seller, and that the Goods manufactured or Services provided by Seller will be free from defects in materials or workmanship under normal use and care until the expiration of the applicable warranty period. Goods are warranted for twelve (12) months from the date of initial installation or eighteen (18) months from the date of shipment by Seller, whichever period expires first.
The right people, the right answers, right now. ON-LINE ORDERING NOW AVAILABLE ON OUR WEB SITE http://www.raihome.com Specifications subject to change without notice. Credit Cards for U.S. Purchases Only. Emerson Process Management Liquid Division 2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250 http://www.raihome.com © Rosemount Analytical Inc.