DOC022.53.00619 Digital Reactor Block 200 (DRB 200) Instrument Manual © Hach Company, 2003. All rights reserved. Printed in Germany.
Table of Contents Safety Precautions................................................................................................5 Specifications ........................................................................................................7 Section 1 Introduction....................................................................................9 1.1 Front Display ..............................................................................9 Operation .......................................
Safety Precautions Please read this entire manual before unpacking, setting up, or operating this instrument. Pay particular attention to all danger and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment. To ensure the protection provided by this equipment is not impaired, do not use or install this equipment in any manner other than that which is specified in this manual.
Safety Precautions Safety Equipment Use protective clothing when operating the reactor, including goggles or face mask, and gloves. Reagent Spills Clean up spilled reagents immediately. If reagent contacts skin, rinse the affected area thoroughly with water. Avoid breathing released vapors. Read the Material Safety Data Sheets (MSDS) supplied with each reagent for complete chemical information. Fire Hazard Avoid the presence of flammable liquids near the operating reactor. A fire hazard could be created.
Specifications Specifications are subject to change without notice. Dimensions 250 x 145 x 310 mm (W x H x D) LTV082.53.30001: 2 kg instrument, 3.5 kg with packaging Weight LTV082.53.40001: 2 kg instrument, 3.5 kg with packaging LTV082.53.42001: 2.8 kg instrument, 4.
Section 1 Introduction The DRB 200 is supplied as two models, with either one or two heating blocks (Figure 1). The heating blocks can heat solutions in round vials of various sizes at 37–165 °C for a period of 0–480 minutes. The small, 16 mm diameter openings on the heating block are suitable for Hach COD, Unicell, TOC, and Test N’ Tube tests. The larger, 20 mm diameter openings are intended for sample preparation reaction vessels, using the Metals Prep Set.
Introduction The actual temperatures of the heating blocks and the remaining time are visible in the display while temperature programs are active. Figure 2 DRB 200 Display and Keys 1 2 1. Display 2.
105°C TOC: OK 120’ 120’ 60’ 105°C: 105°C OK 60’ 60’ 165°C: 165°C OK 60’ 150°C: 150°C OK Select program PRG1 PRG2 Digestion period 120’ 60’ 30’ Select program 150° 165° Digestion period 120’ 60’ 30’ Select program 100° 105° Select program COD TOC Digestion period 120’ 60’ 30’ 100°C: 100°C OK Digestion period 120’ 60’ 30’ 150°C COD: OK TOC Start Select block right left COD Start ? Select program PRG3 Figure 3 Initializing V 1.
Operation DANGER Handling chemical samples, standards, and reagents can be dangerous. Review the necessary Material Safety Data Sheets and become familiar with all safety procedures before handling any chemicals. DANGER La manipulation des échantillons chimiques, étalons et réactifs peut être dangereuse. Lire les Fiches de Données de Sécurité des Produits (FDSP) et se familiariser avec toutes les procédures de sécurité avant de manipuler tous les produits chimiques.
Section 2 Instrument Use 2.1 Starting-up DANGER The ventilation slits in the lid must not be covered, or overheating may occur. Initializing V X.X Figure 4 1. 1. Place the instrument on a stable, level, heat-resistant surface. 2. Plug in the power cord into a power socket (100–230 V +5%/–15%, 50/60 Hz). 3. Switch on the instrument by switching the power switch (Figure 4). 4. After initialization, the instrument will beep once, indicating that it is ready for operation.
Instrument Use Language GB D Language F I 2. Press the right arrow key to scroll through the menu. Select the required language (see Table 1). 3. The instrument is automatically initialized and is then ready for operation. Language E NL Table 1 Language Settings Language S PL 2.1.2 Abbreviation Country GB English D Germany F France I Italy E Spain NL Netherlands S Sweden PL Poland DK Denmark Adjusting the Contrast 1. Hold down the middle key while switching on the instrument.
Instrument Use 5. Place the vials in the appropriate heating block and close the protective lid. 6. Start the program using the left key. 7. The time automatically counts down to zero (0). The actual temperature and the remaining time are visible on the display. Clock Symbol Description The remaining time counts down to zero (0). 8. The instrument will beep three times to indicate the temperature program is complete. It will turn off the heater and cool.
Instrument Use Table 3 Stored Programs Program Description COD Program Select program COD TOC COD: OK 150°C 120’ TOC Program Select program COD TOC TOC: OK 105°C Heats vials for 2 hours at 150 °C. In the cooling phase, 4 beeps indicates that the vials have cooled to 120 °C. Remove and carefully invert the vials several times, before allowing them to cool further in a rack. Heats the vials for 2 hours at 105 °C. This setting is suitable for all Hach TOC vial tests.
Instrument Use Table 3 Stored Programs (Continued) Program Description 165 °C Program Select program 150° 165° Digestion period 120’ 60’ 10’ 165°C: 165°C OK Heats vials for 30, 60, or 120 minutes at 165 °C. 60’ 2.5 Setting User Programs The DRB 200 can accommodate three user programs in storage locations PRG1, PRG2, and PRG3. Select program PRG1 PRG2 1. Select PRG1 from the Select Program menu. 2. Press Prog to enter the programming mode. Program name? (PRG1) OK 3.
Section 3 Maintenance There are no scheduled maintenance requirements for the instrument. To ensure reliable and precise operation, it must be kept clean. 3.1 Cleaning the Instrument DANGER Strong acids and bases can cause burns. 1. Switch off the instrument, unplug the power cord and allow the instrument to cool. 2. Wipe the instrument with a soft, damp cloth. Make sure no water penetrates into the instrument.
Maintenance 1. Fill a clean, empty vial with glycerol at room temperature, and insert the thermometer until it touches the bottom of the vial. 2. When the thermometer is in the vial, the level of the glycerol must be 51 mm ± 0.5 mm from the bottom. 3. Insert the vial in the center opening of the second row of the test block. 4. Start the temperature program for 150 °C, 60 minutes (or the COD program) for this block. 5.
General Information At Hach Company, customer service is an important part of every product we make. With that in mind, we have compiled the following information for your convenience.
Parts and Accessories Description Part No. DRB200-1 with 9 holes for 16 mm vials and 2 holes for 20 mm vials ....................................................LTV082.53.30001 DRB200-1 with 15 holes for 16 mm vials .....LTV082.53.4001 DRB200-2 with 21 holes for 16 mm vials and 4 compartments for 20 mm vials ..................LTV082.53.4200 Operating Manual US Version .................. DOC022.53.00619 Operating Manual EU Version.................. DOC022.98.00619 Protective Cover Replacement .............
How To Order By Telephone: By Mail: 6:30 a.m. to 5:00 p.m. MST Monday through Friday (800) 227-HACH (800-227-4224) By Fax: (970) 669-2932 Hach Company P.O. Box 389 Loveland, CO 80539-0389 U.S.A. Ordering information by E-mail: orders@hach.com Information Required • Hach account number (if available) • Billing address • Your name and phone number • Shipping address • Purchase order number • Catalog number • Brief description or model number • Quantity Technical and Customer Service (U.S.
Repair Service Authorization must be obtained from Hach Company before sending any items for repair. Please contact the HACH Service Center serving your location. In the United States: Hach Company 100 Dayton Avenue Ames, Iowa 50010 (800) 227-4224 (U.S.A. only) Telephone: (515) 232-2533 FAX: (515) 232-1276 In Canada: Hach Sales & Service Canada Ltd. 1313 Border Street, Unit 34 Winnipeg, Manitoba R3H 0X4 (800) 665-7635 (Canada only) Telephone: (204) 632-5598 FAX: (204) 694-5134 E-mail: canada@hach.
Warranty Hach Company warrants this product to the original purchaser against any defects that are due to faulty material or workmanship for a period of one year from date of shipment. In the event that a defect is discovered during the warranty period, Hach Company agrees that, at its option, it will repair or replace the defective product or refund the purchase price, excluding original shipping and handling charges.
Certification Hach Company certifies this instrument was tested thoroughly, inspected and found to meet its published specifications when it was shipped from the factory. The DRB 200 has been tested and is certified as indicated to the following instrumentation standards: Product Safety: Certified to EN 61010-1 A1 / A2 & EN 61010-2-010 A/1 per 73/23/EEC LVD by TUV (Rheinland) with TUV-GS safety mark. Listed to UL 61010A-1/UL 61010A-2-010 and CSA C22.2 No. 1010.1 A2 and CSA C22.2 No. 1010.2.
Certification, continued test records by REICHL (Report No. 030028) and certified compliance by Hach Company. Standards include: EN 61000-3-2 Harmonic Disturbances Caused by Electrical Equipment EN 61000-3-3 Voltage Fluctuation (Flicker) Disturbances Caused by Electrical Equipment Additional Emissions Standard/s include: CANADIAN INTERFERENCE-CAUSING EQUIPMENT REGULATION, IECS-003, Class A: Supporting test records records by REICHL (Report No. 030028) and certified compliance by Hach Company.
Certification, continued case the user will be required to correct the interference at his own expense. The following techniques of reducing the interference problems are applied easily: 1. Disconnect the Model DRB 200 Digital Reactor Block from it's power source to verify that it is or is not the source of the interference. 2. If the Model DRB 200 Digital Reactor Block is connected into the same outlet as the device with which it is interfering, try another outlet. 3.