Shor t-For m Reminders Short-For t-Form Electrodes - Install/Replace Reagents - Install/Replace Select method/sequence pH electrode calibration Reagent calibration Running methods Running sequences Direct measurements Operations during analyses Manual dosing Maintenance recommendations Storage recommendations Spare parts & accessories Electrodes Calibration standards & solutions D21T047 • Printed by Radiometer Analytical SAS • 2008-09H Short-Form Reminders 1
Short-Form Reminders 2
to ress u s e ! p key s in one c t r o d e y l On h e e l e ck t che Electrodes - Install/Replace Form no. 1 Select method or sequence and 3 For a method XYZ 2 and VW For a sequence Install electrode system 1. 2. 3. Enter Electrode window 2 1 VW STU then 4.
Replace with electrode of same type and ID 1. Enter Electrode window 4. Disconnect old electrode 1 and confirm STU 2. 2 3 VW XYZ then 3. 5. Press ✓ to select electrode Connect new electrode 6. Enter serial no. and confirm Disconnect electrode system 2. Enter Electrode window 2 VW 3. Disconnect electrode and press ✓ to confirm 2 then VW Check electrode system Enter Electrode window 1. 2. 3 XYZ To view parameters Press ✓ to select electrode 3. 4.
s, ottle e b t dur agen ty re ge proce p m an ee plac tle exch e r o t T o the b use Reagents - Install/Replace Form no. 2 Select method or sequence and 3 XYZ For a method and 2 VW For a sequence Install reagent system 1. 2. Enter Reagent window 2 1 VW STU then 3. Press ✓ to enter batch no., expiry date then confirm 4. If required, rinse burette 5. Install reagent bottle and press ✓ to flush Remove a reagent Run the Rinse procedure in the Burette functions screen.
Check reagent system 1. 2. Enter Reagent window 3 XYZ To view parameters Press ✓ to select reagent 3. 4. Esc To return to the reagent window Bottle exchange: with one of same type and ID 1. 2. Enter Reagent window 2 VW then 2 VW 4. 1 Confirm STU 5. Enter batch no. and expiry date of new reagent and confirm 6. Remove bottle 7. Install new bottle and press ✓ to flush and fill Replace reagent: with different type and ID 1. 2. Enter Reagent window 2 VW then 4. Confirm replace 1 STU 5. 3.
ard t f o r w tion h g i S t r a d selec o meth Select method/sequence Form no. 3 Select method 1. Enter main menu 2. 3. Select Method mode 3 Select method from list XYZ 4.
Select sequence Enter main menu 2. 3. Select Sequence mode 2 VW then 4. 5. Enter Sequence ID confirm Esc Check icons You can run the method/sequence You can run the method/sequence. However a calibration and/or a reagent bottle exchange must be performed soon Check the electrodes and reagents for installation or calibration purposes Programming error due to missing parameters D21T047 • Printed by Radiometer Analytical SAS • France • 2008-09H 1.
ode rate Calib r elect your pH electrode calibration Form no. 4 Select electrode 1. Enter Electrode window 2. 1 STU 3. to select electrode from list then Confirm Run 1. 1 STU 2.
3. Rinse electrode(s) and dip in beaker 4. Confirm 5. The measurement starts 1 Calibration can be performed on up to 5 buffers.
ent reag r u yo rate b i l a C Reagent calibration Form no. 5 Select reagent 1. Enter Reagent window 2. 1 STU 3. to select reagent from list then Confirm Run 1. 1 STU 2.
3. Enter Standard batch number and standard amount then confirm 1 STU 4. Rinse electrode(s) and dip in beaker 5.
Run ses naly a r you Running methods Form no. 6 Run 1. 1 STU 2. To run your selected method Enter User ID and temperature, if required, and confirm 1 STU 3. Enter Sample ID, sample amount and confirm 1 STU 4.
Automatic result display Press 1 to save results View statistics 2 VW then 2 VW More tests/End of analysis Emergency stop 1 STU “Resume analysis” D21T047 • Printed by Radiometer Analytical SAS • France • 2008-09H Stop
stack e l p m ur Sa nalyses o y Use daily a for Running sequences Form no. 7 Preparing the sample stack 1. 2 VW + 1 STU 5. Locate beaker no.1 6. 2. Repeat steps 2 to 4 for each beaker in the sequence Enter a new sample ID and confirm 7. 3. Check the sample test quantity or enter the sample test quantity to place in beaker no.1 + 4.
Run 1. 3. Rinse the electrodes, and dip in beaker 1, confirm 1 1 STU STU Enter User ID and temperature, if required, confirm 2. 1 STU Automatic result display (manual) Press 1 to save results View statistics (manual) then 2 VW Emergency stop Stop 1 “Resume analysis” STU SAC Sequence For automatic sample handling, using a sample changer, proceed as follows: 2. 1.
? e tab d o r t ing lec the E ogramm n i r ” A “? your p k Chec Direct measurements Form no. 8 Run 2. 3. Connect the electrode(s). See form no. 1 5 MNO To display measurements Dip electrode(s) in beaker Live measurements To select a connected electrode and display measurements 1 STU Esc To start/stop stirring To stop measurements D21T047 • Printed by Radiometer Analytical SAS • France • 2008-09H 1.
e whil s n o i erat g r o p s runnin e h t o i s rm ysi P e r f o ur anal o y Operations during analyses Form no. 9 Instructions 1. Esc To enter the Edit mode 1 then STU You can change the parameters of the active method/sequence. These changes will be taken into account for the next run. 2.
User action required during analyses 1. 2. To return to analysis window Esc To return to edition window Emergency stop Esc 2. 3. Stop Del then then 2 VW 1 STU To return to the analysis window To resume analysis, if desired. Calculations are not performed To end an analysis and get results. Calculations are performed, if result found. D21T047 • Printed by Radiometer Analytical SAS • France • 2008-09H 1.
of ume l o v et pres follow a r e nd Deliv agent a (time) or me) e r e = f = f(volu m u l l Vo igna s d sure mea Manual dosing Form no. 10 Running the manual dosing 1. Select method. See form no. 3. 2. 3. Enter Reagent menu then 5 MNO . Select reagent and electrode. Enter increment size and addition speed. Enter the maximum volume to dose. Define the type of measurement to perform. Confirm 1 STU . Manual dosing with measurements Adjust size of increments.
Manual dosing with no measurement Adjust size of increments. Manual or automatic addition of increments. Volume dispensed. Direct curve Dispensed volume (in ml) = f(time). 1 STU To add one increment or start/stop adding increments automatically. Displaying direct or derivative curve - Identifying curve points Del Direct or derivative curve. Coordinates of that point of the curve. 1 STU or Stop To quit. Quit manual dosing Stop or Del then 1 STU .
, oval m e r bble r bu r o c e d u r e i a e p urett ush For b n t h e F l ru Maintenance recommendations Form no. 11 Daily Check and maintain electrodes according to manufacturer recommendations. Check that there is no crystallisation at piston level, if so rinse the burette using appropriate solvent to remove crystals. If not sufficient, dismount burette to remove crystals.
Annualy Replace burette stand, 1, 5, 10, 25, 50 ml and the anti-diffusion tip, part. no.956-309. Frequent use or use with aggressive or concentrated reagents occurring crystallisation risks may severely reduce the burette and anti-diffusion tip lifetime and may consequently require to replace them more frequently. Replace burette stand set of 3 tubing, (stands 5, 10, 25, 50 ml, part number X31T115 and stand 1 ml, part number X31T116). Replace damaged burette accessories: bottle stopper, desiccant tubing.
in em t s y ! rs you ndition p e Ke top co tip Storage recommendations Form no. 12 Daily Rinse electrodes and delivery tip throughly with distilled water after use. Store the electrode(s) following the instructions given in the respective operating instructions. Overnight and up to 1 week In case of spillages, clean the exterior surface of the instrument with a soft cloth and tepid water. Avoid the accumulation of excess water around the keyboard area.
at form n i e g erin glanc d r a O at ion Spare parts & accessories Form no. 13 Part no.
Part no.
at form n i e g erin glanc d r a O at ion Electrodes Form no. 14 Part no.
Part no. Type Description Pt-Pt Metal electrodes – Karl Fischer titrations E32M001 M231Pt2 Double platinum wire, 2 banana plugs*** E32M002 M241Pt2-8 Double platinum staples, short cable *** For use with adapter, type BNC-f/2 Banana, part no.
at form n i e g erin glanc d r a O at ion Calibration standards & solutions Form no. 15 Part no. Type Description IUPAC Series pH Standards S11M001 pH 1.679 pH 1.679 ±0.010 at 25°C, 500 ml S11M002 pH 4.005 pH 4.005 ±0.010 at 25°C, 500 ml S11M003 pH 6.865 pH 6.865 ±0.010 at 25°C, 500 ml S11M004 pH 7.000 pH 7.000 ±0.010 at 25°C, 500 ml S11M005 pH 7.413 pH 7.413 ±0.010 at 25°C, 500 ml S11M006 pH 9.180 pH 9.180 ±0.010 at 25°C, 500 ml S11M007 pH 10.012 pH 10.012 ±0.
S16M001 RENOVO•N Normal Cleaning Solution, 250 ml S16M002 RENOVO•X Xtra Strong Cleaning Solution, 250 ml C20C370 KS400 Pepsin in HCl Cleaning Solution, 250 ml C20C380 KS410 Thiourea Solution, 250 ml, for junction cleaning C20C300 KS100 KCl Solution, saturated, 500 ml, for Red Rod & Calomel reference C20C500 KS160 K2SO4 Solution, saturated, 500 ml, for Hg/Hg2SO4 reference C20C310 KS120 KCl Solution, saturated with AgCl, 500 ml, for Ag/AgCl reference S21M001 KCl•C KCl Crystals, 15 g S9
