Instruction Manual

Table of contents
72
Laborota 4000 / 4001 efficient, 4010 / 4011 digital, 4002 / 4003 control 1.02
4.5.4 Mounting the vertical condenser (G3–G6) to the condenser holder ...................... 92
4.5.5 Installing the evaporating flask............................................................................... 93
4.5.6 Adjusting the angle of the evaporating flask .......................................................... 93
4.5.7 Adjusting the immersion depth of the evaporating flask ........................................ 94
4.5.8 Releasing the evaporating flask from the vapour tube........................................... 95
4.5.9 Installing the inlet pipe............................................................................................ 96
4.5.10 Installing the inlet hose........................................................................................... 96
4.5.11 Installing the receiving flask ................................................................................... 97
4.5.12 Connecting cooling water (not G5)......................................................................... 97
4.5.13 Connecting the vacuum.......................................................................................... 97
4.6 Adding distillation material ................................................................................................ 102
4.7 Manual aeration................................................................................................................. 102
4.7.1 Installing/connecting accessories......................................................................... 102
5 Using the Laborota 4000 / 4001 efficient; 4010 / 4011 digital.................................................. 106
5.1 Setting the rotating speed ................................................................................................. 106
5.2 Setting the heating bath temperature................................................................................ 107
5.3 Determining boiling temperature (Laborota 4010 / 4011, optional) .................................. 108
6 Using the Laborota 4002 / 4003 control .................................................................................... 109
6.1 Setting the rotating speed ................................................................................................. 109
6.2 Setting the heating bath temperature................................................................................ 110
6.3 Determining the boiling temperature (with optional boiling temperature sensor) ............. 111
6.4 Controlling the vacuum ..................................................................................................... 111
6.4.2 p const mode........................................................................................................ 112
6.4.3 T auto mode ......................................................................................................... 113
6.4.4 p auto mode ......................................................................................................... 114
6.4.5 Interrupting evacuation......................................................................................... 115
6.4.6 Applying the current value as the setpoint (p const mode only) ......................... 115
6.5 Time functions ................................................................................................................... 115
6.5.1 Duration................................................................................................................ 115
6.5.2 Timer .................................................................................................................... 116
6.6 Managing distillation parameters ...................................................................................... 116
6.6.1 Storing data records............................................................................................. 117
6.6.2 Recalling data records.......................................................................................... 117
6.7 Ramp function ................................................................................................................... 117