IC equiment IC equiment: Dosino Regeneration (6.5330.190) Manual 8.110.
Metrohm AG CH-9100 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com IC equiment IC equiment: Dosino Regeneration (6.5330.190) Manual 8.110.
Teachware Metrohm AG CH-9100 Herisau teachware@metrohm.com This documentation is protected by copyright. All rights reserved. Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above. Documentation in additional languages can be found on http://documents.metrohm.com.
■■■■■■■■■■■■■■■■■■■■■■ Table of contents Table of contents 1 Introduction 1.1 1 Description of the IC equiment: Dosino Regeneration ...... 1 1.2 About the documentation ................................................... 1 1.2.1 Symbols and conventions ........................................................ 1 2 Overview 3 2.1 Parts of the IC equiment: Dosino Regeneration ................ 3 3 Installation 4 3.1 Attaching the bottle cap ......................................................
■■■■■■■■■■■■■■■■■■■■■■ Table of figures Table of figures Figure 1 IV ■■■■■■■■ IC equiment: Dosino Regeneration – Parts .........................................
■■■■■■■■■■■■■■■■■■■■■■ 1 Introduction 1 Introduction 1.1 Description of the IC equiment: Dosino Regeneration The IC equiment: Dosino Regeneration enables the transfer of the regeneration solution for the suppressor by means of a Dosino instead of the peristaltic pump. 1.2 About the documentation This manual describes the installation of the IC equiment: Dosino Regeneration. CAUTION Please read through this documentation carefully before putting the equipment into operation.
■■■■■■■■■■■■■■■■■■■■■■ 1.2 About the documentation WARNING This symbol draws attention to a possible hazard due to heat or hot instrument parts. WARNING This symbol draws attention to a possible biological hazard. CAUTION This symbol draws attention to possible damage to instruments or instrument parts. NOTE This symbol highlights additional information and tips.
■■■■■■■■■■■■■■■■■■■■■■ 2 Overview 2 Overview 2.
■■■■■■■■■■■■■■■■■■■■■■ 3.1 Attaching the bottle cap 3 Installation Proceed as follows to install the IC equiment: Dosino Regeneration: ■ ■ ■ ■ ■ 3.1 Attach the bottle cap to the regeneration solution bottle. Assemble the 800 Dosino and fasten it to the holder. Connect the Dosino to the bottle. Connect the Dosino to the inline filter. Connect the inline filter to the suppressor. Attaching the bottle cap Required accessories ■ ■ ■ ■ ■ Bottle with regeneration solution Eluent bottle cap (6.1602.
■■■■■■■■■■■■■■■■■■■■■■ 3 Installation 3 Mounting the adsorber tube ■ ■ ■ Fill the adsorber tube with some cotton and adsorber material. Place the adsorber tube on the adapter. Insert the adapter into the SGJ opening of the bottle cap. 4 Assembling the bottle cap ■ 3.2 Screw the bottle cap onto the regeneration solution bottle. Mounting the Dosino Attaching the Dosino to the 807 Dosing Unit Required accessories ■ ■ 800 Dosino (2.800.0010) 807 Dosing Unit 2 mL (6.3032.
■■■■■■■■■■■■■■■■■■■■■■ 3.2 Mounting the Dosino 1 Hanging the Dosino holder onto the ion chromatograph ■ ■ ■ Loosen the bottle holder on the ion chromatograph. Clamp the Dosino holder under it. Fasten the bottle holder again. 2 Attaching the Dosino to the holder ■ ■ Place the Dosino onto the Dosino holder. Fasten the Dosino to the Dosino holder by tightening the thread adapter from below.
■■■■■■■■■■■■■■■■■■■■■■ 3.3 3 Installation Connecting the bottle to the Dosino Required accessories FEP tubing (6.1805.120) ■ 1 ■ ■ IC equiment: Dosino Regeneration Tighten one end of the FEP tubing to the M6 opening of the bottle cap. Tighten the other end of the FEP tubing in Port 2 of the Dosino.
■■■■■■■■■■■■■■■■■■■■■■ 3.4 Connecting the Dosino to the inline filter 3.4 Connecting the Dosino to the inline filter Required accessories Inline filter (6.2821.120) Capillary (6.1803.030) Pressure screws (6.2744.070) Coupling M6 / UNF (6.2744.080) Capillary cutter (6.2621.080) ■ ■ ■ ■ ■ 1 ■ Tighten the coupling to Port 1 of the Dosino. 2 ■ Cut off a piece of the capillary that is approx. 30 cm long using the capillary cutter.
■■■■■■■■■■■■■■■■■■■■■■ 3.5 3 Installation Connecting the inline filter to the suppressor Required accessories Pressure screw (6.2744.070) ■ 1 IC equiment: Dosino Regeneration ■ Tighten the capillary of the suppressor labeled regenerant to the outlet of the inline filter using a pressure screw.
■■■■■■■■■■■■■■■■■■■■■■ 4.1 Inline filter 4 Operation and maintenance 4.1 Inline filter The filter has to be replaced at least every 3 months, but if you are working with high backpressure, then it has to be replaced more frequently. Information on replacing the filter can be found in the manual for the ion chromatograph. 4.2 Dosing unit (6.3032.120) Maintenance work on the dosing unit has to be performed regularly.
■■■■■■■■■■■■■■■■■■■■■■ 5 Accessories 5 Accessories Up-to-date information on the scope of delivery and optional accessories for your instrument can be found on the Internet. NOTE When you receive your new instrument, we recommend downloading the accessories list from the Internet, printing it out and keeping it together with the manual for reference purposes.
■■■■■■■■■■■■■■■■■■■■■■ The Partslists webpage will be displayed. 7 Select the desired output language. 8 With the article number entered, click on the command Generate PDF. The PDF file with the accessories data will be created in the language selected. Direct access for all instruments If you are unable to find your instrument using the search as described above, this may be due to the instrument not being sold anymore.
■■■■■■■■■■■■■■■■■■■■■■ Index Index B Bottle cap Installation ........................... 4 D Dosing unit Maintenance ...................... 10 Dosino Mount .................................. 5 IC equiment: Dosino Regeneration I Inline filter Maintenance ...................... 10 Installation Bottle cap ............................. 4 Capillary connection ......... 8, 9 Tubing connection ................ 7 M Maintenance Dosing unit ......................... 10 Inline filter ..........................