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5000 Series Multiple Reactor System TABLE OF CONTENTS Customer Service............................. 2 Related Instruction ........................... 2 Related Instructions The following Parr publications are also available to further your understanding of this instrument and its component parts: Preface ............................................ 3 Scope ........................................... 3 Safety Information ........................ 3 General Specifications .................
5000 Series Multiple Reactor System PREFACE General Specifications Scope Electrical Ratings These instructions describe the installation, operation, and maintenance of the Parr Series 5000 Multiple Reactor System. They cover the basic steps to be followed for installing this system and describe the function of all standard components. They are intended to be used in conjunction with several related instruction sheets listed in the Table of Contents.
5000 Series Multiple Reactor System Explanation of Symbols I On position, half power heater switch O Off position ~ Alternating Current (AC) This CAUTION symbol may be present on the Product Instrumentation and literature. If present on the product, the user must consult the appropriate part of the accompanying product literature for more information. This CAUTION symbol indicates that the surface may be hot. Protective Earth (PE) terminal.
000 Series Multiple Reactor System prospective user is often faced with the choice between over or under-designed equipment. The hazards introduced by under-designed pressure vessels are readily apparent, but the penalties that must be paid for over-designed apparatus are often overlooked.
5000 Series Multiple Reactor System any material will normally fall off as the temperature is increased. PRESSURE AND TEMPERATURE LIMITS Temperature and pressure limits are also affected by the physical properties and temperature limits of the gaskets and seals used in the vessel, and by any valves, gages, or other fittings attached to the vessel. Obviously, the maximum safe operating pressure of any system can be no higher than that of its lowest rated component.
5000 Series Multiple Reactor System INSTALLATION General Setup Guidelines The Series 5000 Multiple Reactor System requires at least 10 square feet of work space on a sturdy bench or table in a well ventilated area with convenient access to an electric outlet. If the tabletop is not heat resistant it would be ideal to provide an insulated pad on which to set the vessels when hot.
5000 Series Multiple Reactor System INSTALLATION (continued) Diagram 1: Layout Diagram of Multiple Reactor System Connect the external grounding strap between the heater and stirrer assembly. Turn on the power switches located on the front of the controller and the stirrer assembly. If present, make sure the stirrer local/remote switch is in the remote position. If there is no stirrer local/remote switch present on this unit, no adjustment is necessary.
5000 Series Multiple Reactor System - 300 °C range. Normally this extrusion doesn’t preclude reuse of the gasket; the extruded portion should be removed with a sharp knife. However, when the gasket thickness is reduced to half of its original thickness, it should be replaced. SOFTWARE INSTALLATION AND OPERATION Installation instructions are listed on the 477M CD which accompanied the 5000 MRS System as "MRS_ReadMe.htm".
5000 Series Multiple Reactor System PARTS LIST Please see Diagrams section for additional parts.
5000 Series Multiple Reactor System PARTS LIST (continued) Rupture disc parts: 526HCPD Rupture disc, 1000 psi 526HCPF Rupture disc, 2000 psi 526HCPG Rupture disc, 3000 psi 581HCPD Rupture disc, 1000 psi, gold faced 581HCPF Rupture disc, 2000 psi, gold faced 581HCPG Rupture disc, 3000 psi, gold faced 49HC2* Orifice cone for rupture disc assembly 527HC Orifice ring for rupture disc assembly 433HC4 Rupture disc body 633HC3 Safety body Manifold parts: A525VB A130VB2 A541VB Needle valve, 1/8"NPT x 1/8"T Needle
5000 Series Multiple Reactor System DIAGRAMS Diagram 1: Diagram 2: Diagram 3: Diagram 4: Diagram 5: Diagram 6: Diagram 7: Diagram 8: Layout diagram of 5000 Multiple Reactor System 5050/5051 Vessel body diagram, PTFE seal and O-ring seal 5050 Vessel, head mounted valves, manual inlet 5050 Vessel, head mounted valves, check valve inlet Manifold panel for head mounted valves Manifold panel for remote mounted valves Base assembly with heater and stirrer, 115V Base assembly with heaters and stirring assembly,
5000 Series Multiple Reactor System DIAGRAMS (continued) 5050 Flat Gasket vessel, 75 mL 5050 O-ring seal vessel, 75 mL 5051 Flat Gasket vessel, 45 mL 5051 O-ring seal vessel, 45 mL Diagram 2: 5050/5051 Vessel Flat Gasket and O-ring - 13 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 3: 5050 Vessel, head mounted valves, manual inlet Diagram 4: 5050 Vessel, head mounted valves, check valve inlet - 14 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 5: Manifold panel for head mounted valves - 15 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 6: Manifold panel for remote mounted valves - 16 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 6 (continued): Manifold panel for remote mounted valves - 17 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 7: Base assembly with heaters and stirring assembly, 115V - 18 -
5000 Series Multiple Reactor System DIAGRAMS (continued) Diagram 8: Base assembly with heaters and stirring assembly, 230V - 19 -
PARR INSTRUMENT COMPANY 211 Fifty-Third Street Moline, Illinois 61265 USA 309/762-7716 800/872-7720 Fax 309/762-9453 http://www.parrinst.com E-Mail: parr@parrinst.