378M 5100 Low Pressure Reactors Operating Instruction Manual
5100 Low Pressure Reactors Preface 3 Scope 3 Related Instructions 3 Intended Usage 3 Safety Information 3 General Specifications 3 Explanation of Symbols Do Not Overfill the Vessel 11 Releasing Pressure 11 Withdrawing Liquid Samples 11 Initial Operating Test 11 Maintenance 12 4 General Maintenance Notes 12 Unpack Carefully 4 Periodic Pressure Tests 13 Provisions for Lifting and Carrying 4 Technical Support 13 Cleaning & Maintenance 4 Us
5100 Low Pressure Reactors Preface Safety Information Scope These instructions describe the installation, operation and maintenance of Parr Series 5100 Fixed Head Bench Top Reactors offered in six sizes from 160 mL to 1.5 L with glass and/or metal cylinders. They cover the basic steps to be followed for installing these reactors and describe the function of all standard components. They are intended to be used in conjunction with several related instruction sheets listed on the previous page.
5100 Low Pressure Reactors Explanation of Symbols II On position, full power heater switch I On position, half power heater switch O Off Position ~ Alternating Current (AC) This CAUTION symbol may be present on the Product Instrumentation and literature. If present on the product, the user must consult the appropriate part of the accompanying product literature for more information. This CAUTION symbol indicates that the surface may be hot. Protective Earth (PE) terminal.
100 Low Pressure Reactors Users Responsibility All Parr reactors and pressure vessels are designed and manufactured with great care to assure safe operation when used within their prescribed temperature and pressure limits. But… the basic responsibility for safety when using this equipment rests entirely with the user; who must: 1. Select a reactor or pressure vessel that has the capability, pressure rating, corrosion resistance, and design features that are suitable for its intended use.
5100 Low Pressure Reactors Installation Pressure and Temperature Limits The maximum working conditions for Parr vessels are stamped on the cylinder. No attempt should be made to increase these limits by making alterations or by substituting components which are not recommended by the Parr Instrument Company. It must also be understood that lower pressure and temperature limits may be required for modified reactors and for vessels made of special alloys.
5100 Low Pressure Reactors Carefully bring the flange of the glass cylinder in contact with underside of the reactor head. A lab jack / cork support is provided for 1.0 and 1.5 liter glass reactors. When using the lab jack, bring the cylinder flush with the O-ring in the head, ensuring no stress is put on the glass. Align the major OD of the head with the OD of the cylinder flange. If a jacketed cylinder is being used, orient the cylinder so that the jacket connections are oriented to either side.
5100 Low Pressure Reactors Secure the clamp on the motor cord with the provided screw next to the motor socket for safety purposes. 6. Connect the thermocouple extension wire to both the thermocouple and to the controller in the “Primary Temp Input” position on the rear panel. Insert the thermocouple into thermowell. 7. Connect leads from accessory packages such as tachometer, pressure transducer and high temp cut-off to the designated positions on the back panel of the 4848 Controller. 8.
5100 Low Pressure Reactors Identify the Valves Other Vessel Head Fittings Gas Inlet Valve Safety Rupture Disc The gas inlet valve is easily identified when the vessel is open by noting that it is connected to a dip tube which extends to a point near the bottom of the vessel cylinder. This is an angle valve with an attached fitting which provides a socket for attaching the A495HC pressure hose furnished with the reactor.
5100 Low Pressure Reactors Accessories Air Motor Variable stirring speeds from 100 to 2000 rpm with no spark hazard can be obtained by replacing the standard motor with an air motor. This motor operates on compressed air which must be supplied at 40 psig minimum pressure with at least 10CFM available at that pressure. It is furnished with a speed control valve and oiler, all assembled on a mounting bracket.
5100 Low Pressure Reactors How to use the Vessel Gas Connections Gas connections are dependent on applications. For general usage, use the pressure hose furnished with the reactor. Screw the Type “A” coned pressure fitting into the adapter attached to the gas inlet valve and tighten the compression nut firmly. Do not use any thread dope on the coned fining. The A495HC pressure hose is made of reinforced Nylon which can be used for all noncorrosive gases at pressures up to 2500 psig.
5100 Low Pressure Reactors Maintenance General Maintenance Notes 1. Periodically inspect all electrical wiring and pressure connections for excessive corrosion. Suspect parts should be replaced by components only supplied by Parr Instrument Company. 2. Always use appropriate wrenches on all fittings and valves. Never use pliers or pipe wrenches. 3. Head and cylinder service fixtures are available for convenience and protection of components during maintenance of your reactor. 4.
5100 Low Pressure Reactors Periodic Pressure Tests Technical Support Each cylinder used in a Parr stirred reactor is tested under hydrostatic pressure to the higher of 1.43 times the rated working pressure at room temperature or 1.30 times the rated working pressure corrected for temperature before it is released from the factory. Micrometer caliper measurements are taken during this test to check the deflection of the walls under pressure.
5100 Low Pressure Reactors Parts List *Note: Special material internal parts (not T316) will have a suffix designating the material: CH - Alloy C-276 CA - Titanium CB - Alloy Cb-20 CG - Alloy B-2 CX - Zirconium HZ - PTFE coated T316 (I.e.- a 300 mL Alloy C-276 dip tube would be 832HC31CH) Cylinders* Model No.
5100 Low Pressure Reactors Thermowell and Thermocouple (Continued) Part No. Description For 1000 mL - 1500 mL: 48HC Gasket for thermowell, Silver 48HCFG Gasket for thermowell, Gold plated Silver 265HC7 265HC7HZ 265HC27 265HC27HZ A472E2 A472E3 Thermowell, 1000 mL, T316 Thermowell, 1000 mL, PTFE coated T316 Thermowell, 1500 mL, T316 Thermowell, 1500 mL, PTFE coated T316 Thermocouple, type-J, 1000 mL, grounded Thermocouple, type-J, 1500 mL, grounded Cooling Loop Part No.
5100 Low Pressure Reactors Stirrer Shaft and Impellers Part No. Description For 160 mL - 600 mL: A837HC Propeller, turbine, T316 A837HC5HZ Propeller, turbine, PTFE coated T316 822HC33 Stirrer shaft, 160 mL, T316, 4.99” length 822HC33HZ Stirrer shaft, 160 mL, PTFE coated T316, 4.99” length 822HC44 Stirrer shaft, 215 mL, T316, 5.69” length 822HC44HZ Stirrer shaft, 215 mL, PTFE coated T316, 5.69” length 822HC30 Stirrer shaft, 300 mL, T316, 6.92" length 822HC30HZ Stirrer shaft, 300 mL, PTFE coated T316, 6.
5100 Low Pressure Reactors External Fittings Part No.
5100 Low Pressure Reactors Accessories Part No.
5100 Low Pressure Reactors Product Features and Part Identification 5100 Stand Mini Stand (160 mL - 600 mL) 2221HC BEARING HSG 2187HC BEARING 2226HC SNAP RING 4X SB1932BT06 4X TW19NL 4X TA1632PP06 2657HC4 ENCASEMENT 4X SB2528SC06 4X SW25NL 2658HC3 BACKPLATE 4X SA1632RP06 2222HC5 DRIVE SHAFT 2209HC3 FLEX COUPLING 3452HC3 MIDPLATE 2064EKX .
5100 Low Pressure Reactors Stand for 5100 160 - 600 mL Vessels 1355EES MOTOR 1/8 HP (4) SB1932BT06 (8) SW19FT (4) TW19NL (4) 2186HC 2656HC BELT GUARD 2663HC HINGE, BELT GUARD (3) SA1632RP06 (3) SA1332RP04 (3) SW16FT 2661HC PULLEY 2-STAGE, LD DRIVE 2662HC PULLEY 2-STAGE, HD DRIVE 1564HC OPTICAL WHEEL 1:1 1564HC2 OPTICAL WHEEL 2:1 (3) SA1332RP04 A1001E6 SENSOR ASSY SN1632WG (2) TN1140HL 847HC10 DRIVE BELT 1:1 DRIVE 847HC9 DRIVE BELT 2:1 DRIVE 857HC4 DRIVEN PULLEY X2170A MAG DRIVE SHIELD 2655HC OVERARM PLA
5100 Low Pressure Reactors Stand for 5110 1 L and 1.
5100 Low Pressure Reactors 5100 Overarm Overarm Components, Common For All 5100 Series Reactors 2656HC BELT GUARD 2663HC HINGE 1564HC OPTICAL WHEEL 1700 RPM 1564HC2 OPTICAL WHEEL 850 RPM 2661HC PULLEY, 2 STAGE (1/8 HP MOTOR) 2662HC PULLEY, 2 STAGE (1/4 HP MOTOR) 857HC7 PULLEY (AIR MOTOR) A1001E6 TACH SENSOR ASSY 2655HC OVERARM PLATE (2) 2446HC THUMB SCREWS 847HC10 DRIVE BELT 1700 RPM 847HC9 DRIVE BELT 850 RPM 857HC PULLEY, DRIVEN (FLIP OVER WHEN USING 850 MAX RPM) 2634HC DRIVE ADAPTER A1120HC9 MAG DRIVE A
5100 Low Pressure Reactors 5100 Internals 300 mL - 450 mL Glass Vessels A138CA MALE CONNECTOR (REF) A138CA MALE CONNECTOR (REF) 2635HC3 HEAD 2635HC3 HEAD (3) A92HW MALE CONNECTOR (3) A92HW MALE CONNECTOR A1453HC THERMOWELL 2943HCHZ THERMOWELL, PTFE COATED A472E THERMOCOUPLE (NOT SHOWN) A1453HC THERMOWELL 2943HC2HZ THERMOWELL, PTFE COATED A472E2 THERMOCOUPLE (NOT SHOWN) 832HC31 DIP TUBE 832HC32 DIP TUBE 822HC30 SHAFT, STIRRER 822HC31 SHAFT, STIRRER 831HC7 COOLING LOOP (2) A837HC IMPELLER 831HC6 C
5100 Low Pressure Reactors 5100 Internals (continued) 600 mL Glass Vessels A138CA MALE CONNECTOR (REF) 2635HC3 HEAD NOT SHOWN / COMMON FOR ALL A2526HC SPLIT RING ASSY (GLASS) A2735HC SPLIT RING ASSY (METAL) 2632HC SERIES O-RING (3) A92HW MALE CONNECTOR A1453HC THERMOWELL 2943HC3HZ THERMOWELL, PTFE COATED A472E3 THERMOCOUPLE (NOT SHOWN) 832HC33 DIP TUBE 822HC32 SHAFT, STIRRER 831HC8 COOLING LOOP (2) A837HC IMPELLER A1260HC2 STIRRER BRACKET ASSY PTFE COATED = 1218HC5HZ INNER BRACKET 1219HC5HZ OUTER BRACKET
5100 Low Pressure Reactors 5100 Internals (continued) 160 mL - 215 mL Glass Vessels A138CA MALE CONNECTOR (REF) 2635HC3 HEAD NOT SHOWN: A2526HC SPLIT RING ASSY 2632HC SERIES O-RING A472E THERMOCOUPLE (ALL OTHER HEAD EXTERNALS) A92HW MALE CONNECTOR 822HC33 SHAFT, STIRRER 2525HC4 CYLINDER, GLASS, 160mL A1453HC THERMOWELL 2943HC4HZ PTFE COATED THERMOWELL 832HC35 DIP TUBE A837HC IMPELLER A138CA MALE CONNECTOR (REF) 2653HC3 HEAD 5104 160mL GLASS A92HW MALE CONNECTOR 822HC44 SHAFT, STIRRER 2525HC14 CYLINDER,
5100 Low Pressure Reactors 5111 & 5112 Internals 1 L & 1.5 L Glass Vessels 2915HC2 HEAD NOT SHOWN: A2916HC SPLIT RING ASSY (FOR GLASS) A2912HC SPLIT RING ASSY (FOR METAL) 2913HC SERIES O-RING A472E2 THERMOCOUPLE (1.0L) A472E3 THERMOCOUPLE (1.5L) (3) A92HW MALE CONNECTOR A449HC STIRRER SHAFT ASSY (1.0L) A449HC22 STIRRER SHAFT ASSY (1.5L) 686HC19 DIP TUBE (1.0L) 686HC20 DIP TUBE (1.
5100 Low Pressure Reactors 5100 Metal Vessels Internals 160 mL - 215 mL Vessels A138CA MALE CONNECTOR (REF) 2635HC3 HEAD A92HW MALE CONNECTOR 822HC33 SHAFT, STIRRER 832HC35 DIP TUBE A1453HC THERMOWELL 2943HC4HZ = PTFE COATED A837HC IMPELLER 2630HC4 METAL CYLINDER 160mL NOT SHOWN: A2735HC SPLIT RING ASSY 2632HC SERIES O-RING A472E THERMOCOUPLE A138CA MALE CONNECTOR (REF) 2635HC3 HEAD A92HW MALE CONNECTOR 822HC44 SHAFT, STIRRER 832HC36 DIP TUBE A1453HC THERMOWELL 2943HC5HZ = PTFE COATED A837HC IMPELLER 2630
5100 Low Pressure Reactors 5100 Head Assembly Head Assembly for 160 mL - 600 mL Vessels A92HWAD MALE CONNECTOR TYP (2) PLACES ( W / CO O L I N G L O O P ) 79HWAD PLUG, HEX HEAD TYP (2) PLACES (W/O COOLING LOOP) A888HC2 RUPTURE DISC ASSY 366VBAA H E X CO U P L I N G 288VBAD MALE CONNECTOR 420HC ADAPTER A122VB NEEDLE VALVE 835HC ADAPTER A122VB NEEDLE VALVE A146VB ANGLE VALVE 154VB2 ELBOW, 45 DEGREE * A140VB2P1 RELIEF VALVE OR A693VBP145 RELIEF VALVE (CE) 2634HC DRIVE ADAPTER 2633HCP2AD GAGE 414VB ELBOW,
5100 Low Pressure Reactors 5110 Head Assembly Head Assembly for 1 L & 1.
5100 Low Pressure Reactors 5100 Head Fittings and Valves 2633HCP2AD GAGE 414VB ELBOW A140VB2P1 RELIEF VALVE 154VB2 ELBOW, 45 DEG 836HC7 GAGE ADAPTER A122VB NEEDLE VALVE (GAS RELEASE) 2635HC3 HEAD 5100 PRESSURE GAGE A146VB ANGLE VALVE A122VB NEEDLE VALVE 420HC ADAPTER 835HC ADAPTER 5100 GAS INLET/LIQUID SAMPLING VALVES 5110 Head Fittings and Valves 2633HCP2AD GAGE 414VB ELBOW A146VB ANGLE VALVE 260HC2 VALVE EXTENSION 2915HC2 HEAD A140VB2P1 RELIEF VALVE 154VB2 ELBOW 45 DEG A146VB ANGLE VALVE 420HC ADA
Notes www.parrinst.
378M R06 10/24/14