User Manual

[ CARE AND USE MANUAL ]
CONTENTS
I. INTRODUCTION
II. STANDARD PREPARATION
III. ADDITIONAL RESOURCES
IV. ORDERING INFORMATION
Biopharmaceutical Training Kit
I. INTRODUCTION
The Biopharmaceutical Training Kit is designed to provide trainers
and customers with high quality standards that can be utilized as a
starting point for running biopharmaceutical applications on their
Waters UPLC inlet with Tof or Q-Tof mass spectrometry detection
systems. The training kit pulls together many of the individual
standard samples that are often used in demos and training classes,
including reference compounds for calibration and lockmass. This
kit provides a foundation for biopharmaceutical LC-MS analysis and
can be used for optimization of methods prior to running valuable
samples to ensure system performance and confidence in results.
Table 1. Kit Components for Biopharmaceutical Training Standards (P/N 186006921)
Part # Contents Description of Components Acid
Amount
per Vial
Container
186006921-1 1 x 15 mL Horse Heart Myoglobin 2.5 mg 15 mL Clear Nalgene Bottle
186006921-2 1 vial Intact mAb Mass Check Standard 1 mg
TruView™ Max Recovery with non-slit PTFE/
silicone Septa (p/n 186005668CV)
186006921-3 1 vial Glu-fibrinopeptide B 0.5 mg 4 mL Amber Screw Top Vial
186006921-4 1 vial MassPREP Enolase Digest 1 nmol
TruView Max Recovery with non-slit PTFE/
silicone Septa (p/n 186005668CV)
186006921-5 1 vial Reverse Peptide Ser-Asp-Gly-Arg-Gly 1.0 mg of each 4 mL glass amber bottle with screw top
186006921-6 1 vial Reverse Peptide Gly-Arg-Gly-Asp-Ser 1.0 mg of each 4 mL glass amber bottle with screw top
Table 2. Kit Components for Biopharmaceutical Prep Kit (P/N 186007517)
Part # Contents Description of Components Acid
Amount
per Vial
Container
186007517-1 1 x 2 mL Formic Acid 2 mL 2 mL Ampoule
186007517-2 1 x 30 mL Sodium Cesium Iodide 2 μg/μL 30 mL Nalgene
290002010 3 30 mL Nalgene Fludics Bottle (with cap) Empty 30 mL Nalgene Fludics Bottle (with cap)
The Biopharmaceutical Training Kit comes in two separate boxes. The Biopharmaceutical Training Standard Kit (see Table 1) contains
the standards. This kit is shipped at ambient temperatures, however upon receipt of this kit, please store at -20 °C to maximize long
term stability. The Biopharmaceutical Training Prep Kit (see Table 2) contains the materials needed for solubilization and standard prep.
This kit is shipped at ambient temperatures and can be stored at room temperature. Once any component is opened, use right away for
optimum results.