OPERATIONS MANUAL ba75950e02 11/2012 CarboVis 701 IQ CarboVis 705 IQ OPTICAL SENSOR FOR CARBON SUM PARAMETERSNITRITE, NITRATE AND CARBON SUM PARAMETERS
CarboVis 70x IQ For the most recent version of the manual, please visit www.ysi.com. Contact Copyright 2 YSI 1725 Brannum Lane Yellow Springs, OH 45387 USA Tel: +1 937-767-7241 800-765-4974 Email: environmental@ysi.com Internet: www.ysi.com © 2012 Xylem Inc.
CarboVis 70x IQ Contents CarboVis 70x IQ - Contents 1 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1 1.1 1.2 1.3 1.4 2 Safety . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1 2.1 2.2 3 3.4 11/2012 IQ SENSOR NET system requirements . . . . . . . . . . . . . . 3-1 Scope of delivery of the CarboVis 70x IQ . . . . . . . . . . . 3-1 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-2 3.3.
CarboVis 70x IQ 5 Maintenance and cleaning . . . . . . . . . . . . . . . . . . . . . . .5-1 5.1 5.2 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-1 Sensor cleaning . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5-1 5.2.1 Cleaning agents and accessories . . . . . . . . . . .5-1 5.2.2 General steps to be taken . . . . . . . . . . . . . . . . .5-2 5.2.3 Basic cleaning . . . . . . . . . . . . . . . . . . . . . . . . . .5-3 5.2.4 Cleaning the measuring gap . .
Overview CarboVis 70x IQ 1 Overview 1.1 How to use this component operating manual Structure of the IQ SENSOR NET operating IQ Sensor Net Operating Manual manual System Operating Manual (Ring Binder) IQ Sensor Operating Manual MIQ Module Operating Manual MIQ Terminal Operating Manual Component Operating Manuals Fig. 1-1 Structure of the IQ SENSOR NET operating manual The IQ SENSOR NET operating manual has a modular structure like the IQ SENSOR NET itself.
Overview CarboVis 70x IQ 1.2 Fields of application The CarboVis 70x IQ is an online sensor for the on-site determination of carbon sum parameters (and total suspended solids - TSS) in waste water treatment plants. The CarboVis 70x IQ is an online sensor for the on-site determination of nitrite, nitrate and carbon sum parameters in waste water treatment plants. The range of application comprises control, feedback control and monitoring.
CarboVis 70x IQ Overview The influence of typical interference matrix variants occurring at municipal waste water treatment plants can be eliminated by including the entire absorbance spectrum. With this measuring principle, measuring does not take place continuously but at intervals.
Overview CarboVis 70x IQ 1.4 Structure of the UV-VIS sensor A UV-VIS sensor contains a light source (1), a measuring gap (3) to enable the contact of light with the measuring solution, and a detector (5) to measure the attenuated light beam. The sender of the optical system (2) directs a light beam, the measuring beam (6), through the measuring solution and a second light beam, the reference beam (8), over a distance without measuring solution.
Safety CarboVis 70x IQ 2 Safety 2.1 Safety information 2.1.1 Safety information in the operating manual This operating manual provides important information on the safe operation of the product. Read this operating manual thoroughly and make yourself familiar with the product before putting it into operation or working with it. The operating manual must be kept in the vicinity of the meter so you can always find the information you need.
Safety CarboVis 70x IQ 2.2 Safe operation 2.2.1 Authorized use The authorized use of the CarboVis 70x IQ consists of its use as a sensor in the IQ SENSOR NET. Only the operation and running of the product according to the instructions and technical specifications given in this operating manual is authorized (see chapter 8 TECHNICAL DATA). Any other use is considered unauthorized. 2.2.
Commissioning CarboVis 70x IQ Software statuses of the controller and terminal components For cleaning with compressed air via a relay 3 Commissioning 3.1 IQ SENSOR NET system requirements The operation of the CarboVis 70x IQ requires the following software versions in the IQ SENSOR NET: DIQ/S 182 Controller software: Version 3.45 or higher MIQ/MC2 Controller software: Version 3.37 or higher MIQ TC 2020 XT Controller software: Version 3.
Commissioning CarboVis 70x IQ 3.3 Installation 3.3.1 Mounting the sensor Note The sensor is an optical precision instrument that is to be protected against shocks. Make sure the distances to the wall, bottom and other installation surroundings are sufficient. If necessary, protect the sensor from hitting with the protective ring provided. Mount any fixing elements only on the stable metal shaft. Note Always make sure the surface of the enclosure is not damaged by sharp-edged objects.
Commissioning CarboVis 70x IQ Vertical installation For vertical installation, mount the sensor in a position that allows interfering elements in the measuring gap to escape with the current. In the case of vertical installation, the minimum flow rate is 0.2 m/s so the measuring gap is kept clean optimally. Flo easuring gap opening wd ire ctio n Fig. 3-2 Protection against shocks When installing the sensor, always make sure it cannot knock against a wall or another obstacle.
Commissioning CarboVis 70x IQ 3.3.2 Mounting the shock protectors The shock protectors consist of two rings, a cap and four cable ties. To mount the shock protectors, proceed as follows: 3 1 2 Sensor with mounted shock protectors Fig. 3-4 3-4 Mounting the shock protectors 1. Plug the cap (pos. 2 in Fig. 3-4) on one of the two rings (pos. 1). 2. Put the assembled unit on the sensor end and fix it with 2 cable ties (pos. 3) as shown in Fig. 3-4. 3.
Commissioning CarboVis 70x IQ 3.3.3 Connection cable Connecting the sensor to the IQ SENSOR NET A sensor connection cable of the SACIQ or SACIQ SW type is required to connect the sensor. The cable is available in different lengths. Compared to the standard model SACIQ, the SACIQ SW sensor connection cable is optimized regarding its corrosion resistance in seawater and brackish water and adapted for use in conjunction with the CarboVis 70x IQ .
Commissioning Connecting the sensor to the sensor connection cable CarboVis 70x IQ 1. Take the protective caps off the plug connections of the sensor and the SACIQ (SW) sensor connection cable and keep them safe. 2. Plug the socket of the SACIQ (SW) sensor connection cable onto the plug head connector of the sensor. At the same time, rotate the socket so that the pin in the plug head connector (1) clicks into one of the two holes in the socket. 3.
Commissioning CarboVis 70x IQ 3.4 Initial commissioning 3.4.1 General information CAUTION Never look into the measuring window or put objects into the measuring window during operation! The emitted UV radiation can damage the eyes! In the case of authorized use, inadvertent eye contact with the light beam is not possible. Measuring location The sensor is prepared for operation in the outlet of the waste water treatment plant and calibrated in the factory.
Commissioning CarboVis 70x IQ 3.4.2 Sensor structure The physical sensor is the sensor with the instrument or model designation, CarboVis 70x IQ. The physical sensor processes the measurement signal (absorbance spectrum) and supplies up to 5 measurement results to the IQ SENSOR NET. The measurement results are administrated like 5 sensors that differ in hierarchy as follows: Main sensor The sensor for carbon measurement is the main sensor.
Commissioning CarboVis 70x IQ 3.4.3 Measuring cycle Settings for the main sensor A measuring cycle consists of the cleaning procedure, the adjustment time for the measuring system and the determination of the measured value. The following graphic demonstrates the relevant settings: Cleaning Measurement Adjustment time Measuring cycle Time Measuring interval Fig.
Commissioning CarboVis 70x IQ Menu item Settings Explanations Measuring mode COD spectr., total The measured parameter is displayed in the selected citation form. COD spectr., dissolv TOC spectr., correl. BOD spectr., correl. DOC spectr., correl.
Commissioning CarboVis 70x IQ Menu item Settings Explanations Signal smoothing On Switching on/off the signal smoothing. For more details, see Response time Off t90. Response time t90 10 ... 60 min Response time of the signal smoothing. Depending on the sample matrix, measured values can vary more or less strongly (e.g. due to foreign bodies or air bubbles). The signal filter (here, the Response time t90) reduces the limits of variation of the measured values.
Commissioning CarboVis 70x IQ 3.4.4 Carrying out settings Settings for virtual sensors Using , switch from the measured value display to the main menu of the settings. Then navigate to the setting menu (setting table) of the sensor. The procedure is described in detail in your IQ SENSOR NET system operating manual. Default values are marked in bold. Menu item Settings Explanations Measuring mode NO3-N The measured parameter is displayed in the selected citation form.
Commissioning CarboVis 70x IQ Menu item Settings Cal - # raw value 1 Value pairs of the user calibration (see section 4.3.2). Note: Leave those values unchanged during the initial commissioning. Cal - ref. value 1 Explanations Cal - # raw value 2 Cal - ref. value 2 Main sensor Information that there are further sensor overlapping settings in the setting menu of the relevant main sensor (Meas. interval, Cleaning duration, Signal smoothing etc.).
Commissioning 3 - 14 CarboVis 70x IQ ba75950e02 11/2012
Measuring / Operation CarboVis 70x IQ 4 Measuring / Operation 4.1 Determination of measured values Physical sensor, series number xxx Absorbance spectrum of zero adjustment Absorbance spectrum of measurement Main sensor software Virtual sensor software Main sensor meas. mode (algorithm) Virtual sensor meas. mode (algorithm) Main sensor raw value Virtual sensor raw value User calibration data of main sensor User calibration data of virtual sensor Meas. value of main sensor Meas.
Measuring / Operation CarboVis 70x IQ 4.2 Measuring operation CAUTION Never look into the measuring window or put objects into the measuring window during operation! The emitted UV radiation can damage the eyes! In the case of authorized use, inadvertent eye contact with the light beam is not possible. Measured value display Raw value, identifiable by # Measured value Raw value, identifiable by # Measured value Fig.
Measuring / Operation CarboVis 70x IQ ultrapure water The user calibration is not representative (or erroneous) ba75950e02 11/2012 4-3
Measuring / Operation CarboVis 70x IQ 4.3 Calibration 4.3.1 Overview In the delivery condition, the sensor is precalibrated and ready to measure (see section 3.4.1). There are two types of calibration that are included into the calculation of the measured value at different points (see section 4.1): User calibration (see section 4.3.2) Sensor check/Zero adjustment (see section 4.3.3). An overview diagram of the calibration procedures can be found on page 4 - 10.
CarboVis 70x IQ Sensor check (H2O dest.) Measuring / Operation The characteristics of a sensor and thus the measured values provided by it change in the course of time. The reasons for this can be the aging of the sensor, or contamination or mechanical damage of the sensor. Contamination or mechanical damage in the area of the measuring chamber or on the measurement windows affect the measured values.
Measuring / Operation CarboVis 70x IQ 4.3.2 Calibration points and value pairs User calibration The adjustment is carried out at one or two points within the measuring range. A value pair is determined at each point. Each value pair consists of the raw value of the UV-VIS sensor and the corresponding reference value. Each value pair has to be determined at the same time and place as the test sample as possible.
Measuring / Operation CarboVis 70x IQ Performing a user calibration Proceed as follows if you want to perform a user calibration: In the Settings of sensors and diff. sensors menu, set the Signal smoothing setting to Off. Subsequently, leave the menu with Save and quit. How to navigate to the Settings of sensors and diff. sensors menu and the operation of the menu is described in section 3.4.3. 1. Bring the sensor into the measuring position. 2. Switch to the measured value display with . 3.
Measuring / Operation CarboVis 70x IQ Default values are marked in bold. Menu item Settings Explanations Cal - # raw value 1 0.00 ... 5000.00 Raw value of the first value pair (lower concentration). For single-point calibration, enter 0. Cal - ref. value 1 0.00 ... 5000.00 Reference value of the first value pair (lower concentration). For single-point calibration, enter 0. Cal - # raw value 2 0.00 ... 10.00 ... 5000.
Measuring / Operation CarboVis 70x IQ 4.3.3 Sensor check/Zero adjustment Note The sensor check or Zero adjustment must be carried out under absolutely clean conditions. If you do not work carefully enough the Zero adjustment can deteriorate the measuring quality. Ultrapure water (H2O dist.) Storage location of the Zero adjustment data Steps As ultrapure water exclusively use distilled or deionized water that is suitable for analysis purposes.
Measuring / Operation Flowchart CarboVis 70x IQ Cleaning the sensor Sensor check (H2O dist.) Assessment number -40 ...
Measuring / Operation CarboVis 70x IQ Preparing the sensor check or Zero adjustment Prepare the sensor check or Zero adjustment as follows: 1. Switch to the measured value display with . 2. Use <> to select the UV-VIS sensor. 3. Call up calibration with . The Maintenance condition: Linked outputs are frozen. window appears. Fig. 4-4 Maintenance condition By activating the maintenance condition, linked outputs remain in their present state.
Measuring / Operation CarboVis 70x IQ Measuring chamber Sensor sleeve Fig. 4-5 Putting the sensor sleeve on the sensor 9. Put the sensor in a horizontal position on a firm and vibrationfree surface. Turn the filling opening of the sensor sleeve upward (Fig. 4-5). 10. Rinse the measuring chamber with ultrapure water at least 3 times. 11. For Sensor check (H2O dest.) or Zero adjustment: Fill the measuring chamber with ultrapure water.
Measuring / Operation CarboVis 70x IQ 15. Confirm each checklist with until the Start measurement display appears. Up to this point, you can break off the calibration procedure at any time with the key. The system continues to work with the old calibration data. The maintenance condition, however, has to be switched off again in any case. After starting the calibration with the key (step 16.) you can no longer cancel the calibration procedure. 16. Result after Sensor check (H2O dest.
Measuring / Operation CarboVis 70x IQ If no valid zero adjustment is possible under the current conditions, you can restore the readiness for measurement by measuring with an older valid zero adjustment. To do so, select the Zero adjustment setting in the sensor settings Factory (factory zero adjustment) or User (last valid user zero adjustment). Then check the measurement results with a Sensor check (standard).
Maintenance and cleaning CarboVis 70x IQ 5 Maintenance and cleaning 5.1 Maintenance The UV-VIS CarboVis 70x IQ sensor operates maintenance-free. Cleaning agents 5.2 Sensor cleaning 5.2.1 Cleaning agents and accessories To clean the sensor, use the following cleaning agents only: Contamination Cleaning agents Water-soluble substances – Primary cleaning: Tapwater, warm if possible (30 - 50 °C) – Precision cleaning: Household washing-up liquid + ultrapure water.
Maintenance and cleaning CarboVis 70x IQ 5.2.2 General steps to be taken Depending on the application site and the level of contamination of the sensor as well as the coming job, the cleaning procedure includes the following parts: Every cleaning procedure starts with a basic cleaning. It removes tough grime such as incrustation of fouling matter, algae and biological deposits. If the sensor surface might be contaminated with pathogenic germs it should also be disinfected.
Maintenance and cleaning CarboVis 70x IQ Steps of the basic cleaning 5.2.3 Basic cleaning 1. Take the sensor out of the test sample and remove any solid matter deposits and incrustation of fouling matter manually with a brush or sponge. 2. Wash the sensor down with warm tapwater (30 - 50 °C). Note: Do not use a pressure washer or steam blaster. 3. If the sensor might be contaminated with pathogenic germs it should be disinfected with a surface disinfectant.
Maintenance and cleaning CarboVis 70x IQ 5.2.4 Cleaning the measuring gap To remove lime or grease deposits, use the flocked cleaning cards together with the following detergents: Proceeding Contamination Cleaning agents Lime deposits Hydrochloric acid 5 % for analysis Grease deposits Mixture of isopropanol and water (approx. 70 % isopropanol), made of 7 volume parts isopropanol for analysis and 3 volume parts ultrapure water Start by removing any lime deposits.
Spare parts, maintenance equipment, accessories CarboVis 70x IQ 6 General accessories, replacement parts Spare parts, maintenance equipment, accessories Description Model Order no. Calibration sleeve VIS/CV 481 074 20 flocked cleaning cards for cleaning the measuring gap VIS/CT 481 071 Cleaning set: – 20 flocked cleaning cards VIS C/SET 481 079 Description Model Order no.
Spare parts, maintenance equipment, accessories Mounting accessories CarboVis 70x IQ Description Model Order no. Mounting set for horizontal installation with EH/F 170 swing mounting assembly VIS Set/EH 481 073 Flow-through armature VIS FT-1 480 080 Information on other IQ SENSOR NET accessories is given in the WTW catalog and on the Internet.
What to do if... CarboVis 70x IQ 7 "----" display (invalid measured value) What to do if... Cause Remedy – User calibration values entered incorrectly – Correct the entry and enter once again (section 4.3.2) Repeat * Sensor check (H2O dest.) or * Zero adjustment or * Sensor check (standard). * Sensor check (H2O dest.) or * Zero adjustment or * Sensor check (standard) defective Implausible measured values Check conditions, especially cleanliness (section 4.3.
What to do if... Drifting measured values CarboVis 70x IQ Cause Remedy – Cleaning efficiency too low measurement windows becoming more and more contaminated – Clean the measurement windows (section 5.2.4) – Use other cleaning method – Select different measurement location – Set longer cleaning duration – Set more frequent cleaning procedures – Install optional compressed air cleaning device – Failure of the optional compressed air cleaning system – Clean the measurement windows (section 5.2.
What to do if...
What to do if...
Technical data CarboVis 70x IQ Measuring principle Wavelength range 8 Technical data 8.1 Measurement characteristics Spectrophotometric absorption measurement; integrated microprocessor electronics, shielded 2-wire connection for power and data transmission. 200 - 720 nm 200 - 390 nm Measuring gap (optical layer thickness) Carbon measurement, 1 mm gap width CarboVis 701 IQ 1 mm CarboVis 705 IQ 5 mm Measuring location Measuring mode Measuring range Resolution Inlet COD spectr., total 0 ..
Technical data 8-2 CarboVis 70x IQ Measuring location Measuring mode Measuring range Resolution Outlet COD spectr., total 0 ... 4000 mg/L 1 mg/L COD spectr., dissolv 0 ... 4000 mg/L 1 mg/L TOC spectr., correl. 0 ... 2500 mg/L 1 mg/L DOC spectr., correl. 0 ... 2500 mg/L 1 mg/L BOD spectr., correl. 0 ... 2500 mg/L 1 mg/L SAC 254, total 0 ... 3000 1/m 1 1/m SAC 254, dissolved 0 ... 3000 1/m 1 1/m UVT 254 0.0 ... 100.0 % 0.
Technical data CarboVis 70x IQ Carbon measurement, 5 mm gap width Nitrite/nitrate measurement 1 mm gap width Measuring location Measuring mode Measuring range Resolution Outlet COD spectr., total 0.0 ... 800.0 mg/L 0.1 mg/L COD spectr., dissolv 0.0 ... 800.0 mg/L 0.1 mg/L TOC spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L DOC spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L BOD spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L SAC 254, total 0.0 ... 600.0 1/m 0.1 1/m SAC 254, dissolved 0.
Technical data Carbon measurement, 1 mm gap width CarboVis 70x IQ Measuring location Measuring mode Measuring range Resolution Inlet COD spectr., total 0 ... 20000 mg/L 1 mg/L COD spectr., dissolv 0 ... 12500 mg/L 1 mg/L TOC spectr., correl. 0 ... 20000 mg/L 1 mg/L DOC spectr., correl. 0 ... 12500 mg/L 1 mg/L BOD spectr., correl. 0 ... 8000 mg/L 1 mg/L SAC 254, total 0 ... 5000 1/m 1 1/m UVT 254 0 ... 100.0 % 0.1 % COD spectr., dissolv 0 ... 12500 mg/L 1 mg/L DOC spectr.
Technical data CarboVis 70x IQ Carbon measurement, 5 mm gap width Measuring location Measuring mode Measuring range Resolution Outlet COD spectr., total 0.0 ... 800.0 mg/L 0.1 mg/L COD spectr., dissolv 0.0 ... 800.0 mg/L 0.1 mg/L TOC spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L DOC spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L BOD spectr., correl. 0.0 ... 500.0 mg/L 0.1 mg/L SAC 254, total 0.0 ... 600.0 1/m 1 1/m UVT 254 0.0 ... 100.0 % 0.
Technical data Immersion depth Operating position 8-6 CarboVis 70x IQ min The measuring gap must be filled with test sample.
Technical data CarboVis 70x IQ 8.3 Dimensions (in mm) General data 865 hock protection: 891 774 381 Ø 96 Ø 60 Socket SACIQ... With shock protection: 891 120 Ø 96 Weight Connection technique Materials Storage temperature ba75950e02 11/2012 Approx. 3.8 kg (without shock protectors and without sensor connection cable) Approx. 4.
Technical data Instrument safety CarboVis 70x IQ Applicable norms – EN 61010-1 – UL 61010-1 – CAN/CSA C22.2#61010-1 – IEC 62471 Test certificates cETLus, CE Conforms to ANSI/UL 61010-1 Certified to CAN/CSA C22.2#61010-1" 2001759 8.4 8-8 Electrical data Nominal voltage Max.
Indexes CarboVis 70x IQ 9 Indexes 9.1 Explanation of the messages This chapter contains a list of all the message codes and related message texts that can occur in the log book of the IQ SENSOR NET system for the CarboVis 70x IQ. Information on the contents and structure of the log book and the structure of the message code is given in the LOG BOOK chapter of the IQ SENSOR NET system operating manual. The last three digits of the message code form the component code.
Indexes CarboVis 70x IQ 9.1.
Indexes CarboVis 70x IQ Message code Message text ES5541 Failure optical measurement: hardware * Contact service ES6541 Failure optical measurement: software * Contact service ES7541 Failure optical measurement: software BIOS * Contact service ba75950e02 11/2012 9-3
Indexes CarboVis 70x IQ 9.1.2 Info messages Message code Message text IAC541 Zero adjustment was successfully carried out * Carry out sensor check * If required, carry out new user calibration IC3541 The factory zero adjustment was activated. Make sure the sensor operates correctly. IC4541 The last valid user zero adjustment was activated. Make sure the sensor operates correctly. IC5541 Invalid user zero adjustment was replaced by last valid user calibration.
Indexes CarboVis 70x IQ 9.2 Status info The status info is a coded piece of information on the current status of a sensor. Each sensor sends this status info to the controller. The status info of sensors consists of 32 bits, each of which can have the value 0 or 1.
Indexes 9-6 CarboVis 70x IQ ba75950e02 11/2012
Appendix: Glossary CarboVis 70x IQ 10 Appendix: Glossary Resolution Smallest difference between two measured values that can be displayed by a meter. BSB, BOD Abbreviation for the "Biochemical Oxygen Demand". The biochemical oxygen demand of the amount of oxygen required by microorganisms in order to aerobically decompose organic substances in an aqueous solution. CSB, COD Abbreviation for the "Chemical Oxygen Demand".
Appendix: Glossary CarboVis 70x IQ Test sample Designation of the test sample ready to be measured. Measuring gap The measuring gap is between the two measurement windows. In the measuring gap, the light beam penetrates the test sample. Measured value The measured value is the special value of a measured parameter to be determined. It is given as a combination of the numerical value and unit (e. g. 3 m; 0.5 s; 5.2 A; 373.15 K).
CarboVis 70x IQ Contact Information 11 Contact Information 11.1 Ordering & Technical Support Telephone: (800) 897-4151 (937) 767-7241 Monday through Friday, 8:00 AM to 5:00 PM ET Fax: (937) 767-1058 Email: environmental@ysi.com Mail: YSI Incorporated 1725 Brannum Lane Yellow Springs, OH 45387 USA Internet: www.ysi.com When placing an order please have the following information available: YSI account number (if available) Model number or brief description Quantity 11.
Contact Information 11 - 2 CarboVis 70x IQ ba75950e02 11/2012
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